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Novel vitamin E emulsifiable solution and preparation method thereof

A vitamin and emulsion technology, applied in the field of daily chemical technology, can solve problems such as loss of function and loss, and achieve the effects of accelerating the release effect, stabilizing the emulsification system, and being convenient to use.

Active Publication Date: 2012-05-02
广州百花香料股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Because vitamin E is sensitive to oxygen and is easily oxidized, it will decompose slowly in an oxygen-containing environment, and it is also easy to decompose and lose its effect in a strong acid and alkali environment.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0030] The preparation method of novel vitamin E emulsion of the present invention comprises the following steps:

[0031] (1) Weigh the liquid vitamin E, surfactant, solid protector and distilled water according to the weight ratio;

[0032] (2) Preparation of the water phase: add the solid protective substance molecules into distilled water and stir to dissolve or dissolve and completely wet to form an aqueous solution of the protective substance used as the external phase, and set aside;

[0033] (3) Preparation of oil phase: add surfactant to vitamin E to form oil phase used as internal phase, stir to dissolve;

[0034] (4) Put the high-speed shearing machine into the water phase and turn it on. When the speed of the shearing machine is increased to 2000-4000 rpm, slowly add the above oil phase, and after it is completely added, accelerate to 6000-13000 rpm. After 5-15 minutes, reduce the speed of the shearing machine to a complete stop, cool for 20-40 minutes, and then r...

Embodiment 1

[0038] Component Mass / g

[0039] Liquid Vitamin E 10

[0040] Surfactant (sucrose ester) 10

[0041] Solid Preserve (Molecularly Distilled Monoglyceride) 2

[0042] Solid preservative (modified starch) 10

[0043] Solid protectant (β-cyclodextrin) 2

[0044] Solid protection (nano TiO2) 1

[0045]distilled water 65

[0046] The preparation method of novel vitamin E emulsion of the present invention comprises the following steps:

[0047] (1) Weigh according to the above weight ratio: liquid vitamin E, surfactant, solid protective material (molecularly distilled monoglyceride, modified starch, β-cyclodextrin, TiO2), distilled water, and spare;

[0048] (2) Preparation of the water phase: first add the water-soluble solid protective molecule (distilled monoglyceride, modified starch, β-cyclodextrin) into distilled water and stir to dissolve, and then add the insoluble The solid protective substance molecule of water (nano-scale TiO2), fully stirred until it is completely ...

Embodiment 2

[0054] Component Mass / g

[0055] Liquid Vitamin E 5

[0056] Surfactant (sorbitan ester) 20

[0057] Solid Preserve (Molecularly Distilled Monoglyceride) 2

[0058] Solid preservative (modified starch) 10

[0059] Solid protectant (β-cyclodextrin) 2

[0060] Solid protection (TiO2) 1

[0061] distilled water 60

[0062] Preparation method is the same as example one.

[0063] Result analysis: After emulsification, the results of the detected particles meet the test objectives, and the test can be stable in a broad-spectrum (PH 2.5-14) range.

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Abstract

The invention relates to a vitamin E emulsifiable solution and a preparation method thereof. The vitamin oil-in-water type emulsifiable solution provided by the invention is prepared from the following components in weight ratio: 5-35% of liquid vitamin E, 10-20% of solid protector, 5-35% of surfactant and 35-79% of distilled water. According to the vitamin E emulsifiable solution and the preparation method thereof, by adopting the method of mixing the liquid vitamin E, the solid protector, the surfactant and the distilled water in a certain proportion to prepare an O / W-type vitamin E emulsifiable solution having a protection action for a vitamin E, the vitamin E emulsifiable solution can be used in a broad-spectrum (pH 2.5-14) range, and is not damaged or is less damaged so as to maintain the activity of the vitamin E emulsifiable solution, and the approaches for application are wider. Furthermore, the O / W-type vitamin E emulsifiable solution produced by the invention not only can be uniformly dispersed in water in the application, but also has a slow-release action, is extremely convenient to use, and can be widely applied to various cosmetics and other products for daily use.

Description

technical field [0001] The invention relates to the field of daily chemical science and technology, in particular to a novel vitamin E emulsion that can be directly or indirectly used in cosmetics and other daily products and a preparation method thereof. Background technique [0002] Vitamin E (Vitamin E) is a fat-soluble vitamin, also known as tocopheryl acetate, and is one of the most important antioxidants. It has many functions. The more common functions are listed below: [0003] Anti-aging: Vitamin E has the effect of anti-aging, mainly based on its antioxidant capacity. Vitamin E is one of the main biological free radical scavengers and antioxidants in the body. As a fat-soluble vitamin, vitamin E is a chain-breaking antioxidant. Its main function is to block the reaction chain of fat oxidation, and it is the first line of defense against oxidation in the body. The antioxidant effect of vitamin E is located in the cell membrane, which can block the formation of sup...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K8/67C11D3/20C11D7/60C11D9/26A61Q19/00
Inventor 许慧贤马志伟
Owner 广州百花香料股份有限公司
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