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Modified polyactic acid composition for cigarette filter stick and preparation method thereof

A filter rod and polylactic acid technology, which is used in e-liquid filter, application, tobacco and other directions, can solve the problem that the comprehensive adsorption performance is not as good as the acetate fiber filter rod, etc., and achieve the effect of reducing the hazard index, excellent comprehensive performance and fine smoke.

Active Publication Date: 2013-06-19
马鞍山同杰良生物材料有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In terms of filtration and adsorption, the comprehensive adsorption performance is not as good as that of acetate fiber filter rods, and the adsorption performance for some specific harmful substances needs to be improved, such as phenol, hydrogen cyanide, crotonaldehyde, etc.

Method used

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  • Modified polyactic acid composition for cigarette filter stick and preparation method thereof
  • Modified polyactic acid composition for cigarette filter stick and preparation method thereof
  • Modified polyactic acid composition for cigarette filter stick and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0038] Embodiment 1: Modified polylactic acid composition for filter rods

[0039] 1. Composed of:

[0040] composition

Weight (unit: kg)

Polylactic acid (D content 0.5%)

100

Oligolactyl-β-cyclodextrin

1.2

Sodium carbonate

1.0

Sodium pyrrolidone carboxylate

1.0

Vitamin C

0.04

Vitamin E

0.06

polyacrylamide

0.5

[0041] 2. Preparation method:

[0042] 1) Weigh each component, and air-dry the above-mentioned components at 50°C for 8 hours;

[0043] 2) Add all the components into the high-speed mixer according to the dosage, and disperse at a high speed of 500rpm for 30 minutes to obtain a modified mixture;

[0044] 3) The modified polylactic acid composition for tow was obtained by melting and extruding the modified mixture into pellets. The temperature of the twin-screws was controlled at 185° C., and the screw speed was 150 rpm.

[0045] 3. The filter rod prepared by...

Embodiment 2

[0050] Embodiment 2: Modified polylactic acid composition for filter rods

[0051] 1. Subdivided into:

[0052] composition

Weight (unit: kg)

Polylactic acid (D content 0.5%)

100

Oligolactyl-β-cyclodextrin

0.2

Sodium carbonate

0.1

Sodium pyrrolidone carboxylate

0.2

Vitamin C

0.04

Vitamin E

0.06

polyacrylamide

0.5

[0053] 2, preparation method: with embodiment.

[0054] 3. The filter rod prepared by the modified composition was connected to a domestic brand of cigarettes for a comparative test, and the physical routine indicators of the control comparison samples were the same (open draw resistance 1100±30Pa, circumference 24.50±0.1mm). Evaluation methods of main adsorption properties: GB / T5606.1-2004, GB / T16447-2004, GB / T19069-2004, GB / T 23355-2009, GB / T23203.1-2008, GB / T 23356-2009. Please refer to Table 3 for details:

[0055] Table 3: Investigation and Results...

Embodiment 3

[0059] Embodiment 3: Modified polylactic acid composition for filter rods

[0060] 1. Composed of:

[0061] composition

Weight (unit: kg)

Polylactic acid (D content 0.5%)

100

Oligolactyl-β-cyclodextrin

1.2

Sodium carbonate

1.0

Sodium pyrrolidone carboxylate

1.2

Vitamin C

0.04

Vitamin E

0.06

polyacrylamide

0.5

[0062] 2, preparation method: with embodiment 1.

[0063] 3. The filter rod prepared by the modified composition was connected to a domestic brand of cigarettes for a comparative test, and the physical routine indicators of the control comparison samples were the same (open draw resistance 1100±30Pa, circumference 24.50±0.1mm).

[0064] Evaluation methods of main adsorption properties: GB / T5606.1-2004, GB / T16447-2004, GB / T19069-2004, GB / T 23355-2009, GB / T 23203.1-2008, GB / T23356-2009. See Table 4 for the specific evaluation:

[0065] Table 4: Investigation ...

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Abstract

The invention relates to a modified polyactic acid composition for a cigarette filter stick and a preparation method thereof. The composition comprises following parts of raw materials, by weight, 100 parts of polyactic acid, 0.02-3 parts of polyactic acid-beta-cyclodextrin, 0.08-5 parts of sodium carbonate, 0.05-5 parts of sodium pyrrolidonecarboxylate, 0.01-4 parts of vitamin and 0.01-8 parts of polyacrylamide. The filter stick prepared through the polyactic acid composition is better in absorbing performance on smoke compared with the prior art and good in comprehensive performance, and a part of indexes of the filter stick exceed those of a cellulose acetate filter stick.

Description

technical field [0001] The invention relates to the field of chemical industry, in particular to a modified polylactic acid composition for cigarette filter rods and a preparation method thereof. Background technique [0002] The development of filter tip is the product of cigarette development to a certain stage. When the filter first appeared, it was mainly used as a mouth-shaped part of the cigarette for decoration. With the development of cigarette technology and people's pursuit of low-harm cigarettes, the filter has gradually changed from a dispensable position to an indispensable part of cigarettes, and has assumed the function of reducing tar and harm. [0003] Cigarette filters have the functions of filtering, blocking and absorbing harmful components such as nicotine and tar in the smoke. In addition to the above functions, a good filter should also be able to improve the taste of the smoke, reduce the stimulation of the smoke on the mouth and the human body. Hea...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L67/04C08L5/16C08L33/26C08K13/02C08K3/26C08K5/3415B29B9/06B29C47/92D01F6/92D01F1/10A24D3/08B29C48/92
Inventor 王秦峰许克强吕效东
Owner 马鞍山同杰良生物材料有限公司
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