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Synthesizer of imidazolium ionic liquids and application thereof

A technology of ionic liquid and synthesis device, which is applied in the synthesis device and application field of imidazole ionic liquid, can solve the problems of high application cost, low synthesis efficiency, long synthesis time, etc., and achieve simple device, low processing temperature and easy implementation Effect

Active Publication Date: 2014-05-28
AOWEI TIANJIN ENVIRONMENTAL PROTECTION TECH
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  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

However, the synthesis of ionic liquids is the main problem currently encountered. Due to the long synthesis time, it usually takes more than 10 hours, the synthesis efficiency is low, and the yield is low, resulting in high application costs.

Method used

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  • Synthesizer of imidazolium ionic liquids and application thereof

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Embodiment

[0015] A synthesis device for imidazole ionic liquids, comprising a reactor 1, a collection bottle 2, a magnetic stirring heating device 3, an imidazole component raw material bottle 4 and a volatile component raw material bottle 5, and the reactor 1 is a cylindrical sealed container , the wall of the reactor 1 is provided with a heat exchange interlayer 6 and a hot water pipe inlet 7 and a hot water pipe outlet 8 are respectively provided on the lower and upper parts of the heat exchange interlayer, and the top of the reactor 1 is provided with a volatile component discharge port 9. The bottom of the reactor is provided with a liquid discharge port 10, and the reactor 1 is provided with a temperature measuring device sensor probe a11; the liquid discharge port of the reactor 1 is tightly connected with the collection bottle 2, and the magnetic stirring heating device 3 is arranged at the bottom of the collection bottle At the bottom, the magnetic stirrer 12 is located in the c...

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Abstract

The invention discloses a synthesizer of imidazolium ionic liquids. The synthesizer comprises a reactor, a collecting bottle, a magnetic stirring heating unit, an imidazole component raw material bottle and a volatile component raw material bottle, wherein the wall of a reactor is provided with a heat transfer interlayer; the reactor is internally provided with a sensor probe a of temperature measuring equipment, the magnetic stirring heating unit is arranged at the bottom of the collecting bottle, and the collecting bottle is internally provided with a sensor probe b of the temperature measuring equipment; the imidazole component raw material bottle is connected with the reactor and is provided with a liquid delivery pump a, and the outlet end of the imidazole component raw material bottle is provided with an atomization device a; and the volatile component raw material bottle is connected with the reactor and is provided with a liquid delivery pump b, and the outlet end of the light-volatile component raw material bottle is provided with an atomization device b. The synthesizer is used for preparing ion liquid used for extracting cellulose from lignocellulose biomass. The synthesizer is simple and easy to implement, the process for preparing an imidazole ion liquid is simple, the processing temperature is low, the condition is gentle, the substances in a system is utilized in a circulating manner, the raw material utilization ratio is improved, and the rapid and efficient synthesis of the ion liquid is realized.

Description

technical field [0001] The invention relates to the synthesis and application of an ionic liquid for treating biomass, in particular to a synthesis device and application of an imidazole ionic liquid. Background technique: [0002] With the progress of society and the improvement of people's living standards, the people's requirements for the environment are getting higher and higher. Due to the large-scale greening, a large amount of biomass such as branches, leaves, and grass are produced during the maintenance process; at the same time, a large amount of straw-like agricultural waste is produced during agricultural production. At present, most of these lignocellulosic biomass are treated by roadside incineration. On the one hand, it causes serious air pollution. Especially in winter, random burning of lignocellulosic biomass is the main factor causing smog; Smoke seriously affects traffic safety; in addition, burning straw can easily cause fires, which seriously threaten...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/26B01J4/00C07D233/58
Inventor 李维尊鞠美庭刘益良刘乐江洋侯其东王雁南
Owner AOWEI TIANJIN ENVIRONMENTAL PROTECTION TECH
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