A combined process of inferior heavy oil and hydrotreating
A low-quality heavy oil and processing technology technology, applied in the field of hydrogenation, can solve problems such as short operation cycle, and achieve the effect of reducing pressure drop, realizing long-term operation, and slowing down the rising speed.
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Embodiment 1
[0035] Embodiment 1 (the concentration % is mass %)
[0036] The properties of feedstock oil A and feedstock B used in the test are listed in Table 1. This example is an implementation scheme for the hydroprocessing of inferior raw materials, and the schematic diagram of the operation flow is referred to figure 1 .
[0037] Table 1 Main properties of test raw oil
[0038] raw material name
[0039] The process is as follows: the raw material oil A is mixed with the slurry bed hydrogenation catalyst and then enters the slurry bed pretreatment reactor with hydrogen for pretreatment. After the distillate oil is separated from the pretreatment product, the remaining part enters the hydrogenation treatment unit in two ways. The bottoms of the upflow reactors R-1A and R-1B are in contact with the catalysts of the upflow reactors to carry out iron and decalcification reactions, and the reaction products directly enter the bottom of the upflow reactors R-2 without separat...
Embodiment 2
[0042] Embodiment 2 (the concentration % is mass %)
[0043] In this embodiment, the raw material oil used in Example 1 is replaced with the raw material B shown in Table 1, and the slurry bed catalyst is non-supported Ni 2 The amount of P added was 500 μg / g, and the specific process was the same as in Example 1, but the conditions were changed as shown in Table 3 and Table 4.
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