aqueous suspoemulsion
A suspoemulsion, water-based technology, applied in the field of water-based suspoemulsion products, can solve the problems of high cost, difficult to obtain, complicated production process, etc.
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Embodiment 1
[0101] A suspoemulsion formulation was prepared as follows:
[0102] a) prepare the emulsifiable concentrate of lambda-cyhalothrin phase:
[0103] The active ingredient lambda-cyhalothrin (Jiangsu Youshi Chemistry, Jiangsu Youshi Chemical) was mixed with methyl oleate (Clariant) at room temperature. After standing for 30 minutes, emulsifier EL360 (Clariant) was added and stirred until a homogeneous solution was formed.
[0104]
[0105]
[0106] b) Preparation of dispersed particles of lufenuron (ShanghaiStone, Shanghai Stone) active ingredient in a continuous aqueous phase:
[0107] components
Composition (grams)
Remark
Lufenuron Technical (Shanghai Stone)
5 (according to pure product)
active ingredient
Soprophor BSU(Rhodia)
0.5
Dispersant
Soprophor FLK (Rhodia)
1.5
Dispersant
Propylene glycol (DOW)
4
Rhodopol 23 / W (Rhodia)
0.15
thickener
Silicone oil (Degus...
Embodiment 2
[0112] A suspoemulsion formulation was prepared as follows:
[0113] a) prepare the oil-in-water emulsion of lambda-cyhalothrin EW phase:
[0114] components
Composition (grams)
Remark
Beta-cyhalothrin technical
8 (according to pure product)
active ingredient
Propylene carbonate (Local)
8
Atlox4912 (Croda)
2
Emulsifier
Tween 80 (Croda)
0.3
Emulsifier
[0115] Mix the active ingredient lambda-cyhalothrin with Solvesso 100 at room temperature. It was left to stand for 30 minutes before emulsifier EL360 was added and stirred until a homogeneous solution was formed. Then, the lambda-cyhalothrin EC phase was added to water with high shear to obtain the lambda-cyhalothrin EW phase.
[0116] b) Preparation of dispersed granules of lufenuron in a continuous aqueous phase:
[0117]
[0118] The preparation of concentrated suspensions of lufenuron was carried out in the same general manner a...
Embodiment 3
[0122] A suspoemulsion formulation was prepared as follows:
[0123] a) prepare the emulsifiable concentrate of lambda-cyhalothrin phase:
[0124]
[0125] An emulsifiable concentrate of lambda-cyhalothrin was prepared in the same general manner as described in a) of Example 1.
[0126] b) Preparation of dispersed granules of lufenuron in a continuous aqueous phase
[0127]
[0128] The preparation of concentrated suspensions of lufenuron was carried out in the same general manner as described in b) of Example 1.
[0129] c) Suspoemulsion
[0130] A suspoemulsion was prepared using the same general procedure as described in Example 1 c). The low-temperature storage stability (-5°C), high-temperature storage stability (54°C) and stability upon dilution at 30°C of the suspension were tested.
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