Quality control method for lingxian traumatic injury tablet
A quality detection method and a technology of weight ratio, applied in the field of medicine, can solve problems such as low accuracy and sensitivity, poor reproducibility, and cumbersome operation
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[0048] The present invention will be further described below in conjunction with the examples, but the protection scope of the present invention is not limited to the examples.
[0049] The content of two batches of Lingxian Dieda Tablets was detected according to the following detection method, and determined by high performance liquid chromatography.
[0050] Detection instruments: Elite high performance liquid chromatography, UV1201 ultraviolet detector.
[0051] Chromatographic conditions:
[0052] Chromatographic column: general C18 (200mm×4.6mm, 5μm) liquid chromatography column. The filler is SinoChromODS-BP;
[0053] Mobile phase: acetonitrile-tetrahydrofuran (25:10) mixture (mobile phase A), 0.1mol / L ammonium acetate solution (0.5m1 of glacial acetic acid per 1000ml) mobile phase B. Gradient elution, the flow phase is as follows:
[0054] time (min)
Mobile phase A(%)
Mobile phase B(%)
0
15
85
20
20
80
[0055]...
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