Synergistic insecticidal composition containing paichongding and chlorfenapyr
An insecticidal composition, the technology of pichridam, which is applied in the field of agricultural insecticidal compositions, can solve problems such as environmental pollution, pesticide residues, and increase the cost of pesticides for farmers, and achieve the effects of low cost of pesticides, pollution reduction, and dosage reduction
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Embodiment 1
[0016] Formulation example 1: 15% chlorfenapyr aqueous emulsion
[0017] Piclopyr (active ingredient) 7%
[0018] Chlorfenapyr (active ingredient) 8%
[0019] Trimethylbenzene (solvent) 15%
[0020] Sodium alkylbenzene sulfonate (emulsifier) 8%
[0021] Glycerol (stabilizing antifreeze) 5%
[0022] Water make up to 100%
[0023] 2. Preparation of microemulsion
[0024] Dissolve the active ingredient with a solvent and a co-solvent, add an emulsifier and stir until it becomes transparent as the oil phase, and mix the stable antifreeze with water uniformly as the water phase. Slowly add the oil phase into the water phase and stir for 30-60 minutes to form a microemulsion with good dispersibility.
Embodiment 2
[0025] Formulation Example 2: 20% Pichamid·chlorfenapyr microemulsion
[0026] Pichridam (active ingredient) 8%
[0027] Chlorfenapyr (active ingredient) 12%
[0028] Acetone (solvent) 15%
[0029] DMF (solvent) 5%
[0030] Phenylphenol polyoxyethylene ether (emulsifier) 10%
[0031] Nongru 500# (emulsifier) 5%
[0032] Ethylene glycol (stabilizing antifreeze) 2%
[0033] Water top up to 100%
[0034] 3. Preparation of suspending agent
[0035] The active ingredient, dispersant, wetting agent, thickener and water are uniformly mixed sequentially according to the proportion of the formula, and the suspending agent is obtained after being ground by a sand mill.
Embodiment 3
[0036] Formulation example 3: 30% chlorfenapyr suspension concentrate
[0037] Pichridam (active ingredient) 10%
[0038] Chlorfenapyr (active ingredient) 20%
[0039] Sodium alkylbenzene sulfonate (dispersant) 6%
[0040] Alkylphenol polyoxyethylene ether (wetting agent) 4%
[0041] Xanthan gum (thickener) 0.3%
[0042] Water top up to 100%
[0043] Examples of bioassay and drug efficacy test:
[0044] 1. Indoor toxicity determination of Nilaparvata lugens compounded with chlorfenapyr and chlorfenapyr
[0045] The original drug of the test drug pichamidin was produced by Jiangsu Kesheng Group Co., Ltd., and the original drug of chlorfenapyr was the original drug of Xinyi Yonglong Chemical Co., Ltd. The test method refers to the "People's Republic of China Agricultural Industry Standard NY / T 1154.11-2008". After preparing the mother liquor with acetone, an organic solvent for the original drug, use 0.1% Tuwen-80 aqueous solution to prepare 5 series of mass concentrations...
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