Esterified biological asphalt and preparation method thereof
A technology of bio-asphalt and esterification, which is applied in the direction of fatty acid esterification, chemical processing of tar pitch/petroleum pitch/natural pitch, and selective extraction of tar pitch/petroleum pitch/natural pitch, etc., which can solve the problem of bio-bitumen Aging, restrictions on the promotion and utilization of bio-asphalt, etc., to achieve the effect of small viscosity growth rate, good aging resistance, and accelerated reaction
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Embodiment 1
[0024] Example 1 A preparation method of esterified bio-asphalt
[0025] 1) Mix 600g of switchgrass bio-oil and 90g of 1,2-propanediol, add 3g of molecular sieve HZSM-5, and stir and react at 60°C for 2h;
[0026] 2) Use water to extract step 1) to separate the bio-oil after the catalyst, and after standing for 0.5h, filter and separate the insoluble matter;
[0027] 3) The insoluble matter was subjected to air oxidation treatment in an oven at 80°C to obtain bio-pitch 1.
Embodiment 2
[0028] Example 2 A preparation method of esterified bio-asphalt
[0029] 1) Mix 600g of corn stalk bio-oil and 180g of n-octanol, add 3g of 732-type cation exchange resin, and stir and react at 90°C for 0.5h;
[0030] 2) Use water to extract step 1) to separate the bio-oil after the catalyst, and after standing for 0.5h, filter and separate the insoluble matter;
[0031] 3) The insoluble matter was subjected to air oxidation treatment in an oven at 110°C to obtain bio-pitch 2.
Embodiment 3
[0032] Example 3 A preparation method of esterified bio-asphalt
[0033] 1) Mix 600g rice husk straw bio-oil with 90g 1,2-propanediol, add 18g inorganic acid salt NaHSO 4 , stirred and reacted at 120°C for 0.5h;
[0034] 2) Use water to extract step 1) to separate the bio-oil after the catalyst, and after standing for 0.5h, filter and separate the insoluble matter;
[0035] 3) The insoluble matter was subjected to air oxidation treatment in an oven at 120°C to obtain bio-pitch 3.
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