A kind of preparation method and application of polymer polymerization catalyst
A polymer polymerization and catalyst technology, which is applied in the application of the catalyst and the preparation of polymer polymerization catalysts, can solve the problems that cannot fully meet the requirements, and achieve the effects of low production cost, mild reaction conditions and good stability
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Embodiment 1
[0017] Add 0.55 mol of 1,4-butanediol to the flask, add 0.015 mol of manganese acetate into it, then add 0.067 mol of isopropyl titanate, stir continuously, react at 230°C for 1 hour, then add octanoic acid suboxide 5g of tin, after continuous stirring for 2 hours, 3g of calcium aluminate was added, and the stirring was continued for 2 hours to obtain Catalyst 1.
Embodiment 2
[0019] Add 0.55 mol of 1,4-butanediol to the flask, add 0.015 mol of manganese acetate into it, then add 0.067 mol of isopropyl titanate, stir continuously, react at 220 for 1 hour, then add stannous octoate After stirring continuously for 2 hours, 4 g of calcium aluminate was added, and stirring was continued for 2 hours to obtain catalyst 2.
Embodiment 3
[0021] Add 0.55mol of 1,4-butanediol to the flask, add 0.015mol of manganese acetate into it, then add 0.067mol of isopropyl titanate, stir continuously, react at 220 for 1 hour, then add stannous octoate After stirring continuously for 2 hours, 5 g of calcium aluminate was added, and stirring was continued for 2 hours to obtain catalyst 3.
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