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Preparation method of grape juice Maillard cigarette flavor

A technology of grape juice and spices, applied in the direction of essential oils/spices, tobacco, applications, etc., can solve the problems of monotonous aroma, high sugar cost, and few types of spices, and achieve the effect of comfortable aftertaste and improved taste

Inactive Publication Date: 2015-09-09
HUBEI CHINA TOBACCO IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Some people in China simply react glucose with amino acids to form Maillard reaction products. This kind of spice has few varieties and single aroma, which has limited improvement on the quality of tobacco smoking.
Chinese patents (CN1415717A and CN1175623A) disclose "the method for producing spices with tobacco extract as raw material" and "the preparation method and utilization of tobacco reactant spices". Although this method utilizes the Maillard reaction, due to the single type of sugar added, some sugars are very expensive, and the aroma is difficult to achieve a satisfactory effect, and the source of raw materials is also unstable.
[0005] In a word, so far, the disclosed methods of using Maillard to prepare tobacco flavorings are either complicated in process, high in cost, unstable in source of raw materials, or monotonous in aroma, and unsatisfactory in effect. Therefore, a kind of effective and low-cost Maillard Reaction Tobacco Flavoring Is Very Necessary

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0016] Weigh 250 grape juice, put it into a three-necked flask, add 30 grams of alanine, start stirring, then add 30 grams of ammonia to adjust the pH to 9.7, connect the reflux condenser, heat to 90°C in an oil bath, and keep the temperature constant for 3 hours , The stirring speed is 200 rpm, then the heating is terminated, and the reactant is poured out, which is the product of the present invention. The resulting product exhibits a strong fruity, roasted and nutty aroma. The product was added to blank cigarettes in an amount of 0.8‰ for evaluation, and it was found that the product can significantly increase the smoke concentration, make the smoke soft and delicate, cover up the impurities, and significantly improve the quality of tobacco.

Embodiment 2

[0018] Weigh 250 grams of grape juice, put it in a three-necked flask, add 15 grams of alanine, 15 grams of proline, start stirring, then add 30 grams of ammonia to adjust the pH to 9.7, connect the reflux condenser, and heat it with an oil bath The temperature is kept at 95°C for 3.5 hours, the stirring speed is 200 rpm, then the heating is terminated, and the reactant is poured out, which is the product of the present invention. The obtained product showed a strong fruity aroma and burnt sweet aroma. The product was added to blank cigarettes in an amount of 0.8‰ for evaluation. It was found that the product can significantly improve the taste, comfortable aftertaste, alcohol and smoke.

Embodiment 3

[0020] Weigh 250 grams of grape juice, put it into a three-necked flask, add 40 grams of proline, start stirring, then add 50 grams of propylene glycol, 30 grams of concentrated ammonia water to adjust the pH to 9.7, connect the reflux condenser, and heat to 110°C, constant temperature for 3 hours, stirring speed of 300 rpm, then stop heating, pour out the reactant, which is the product of the present invention. The resulting product showed strong roasting aroma and rice aroma. The product was added to blank cigarettes in an amount of 0.8‰ for evaluation, and it was found that the product can significantly increase the concentration of smoke, cover up the fumes, make the smoke elegant and comfortable, and greatly improve the taste of cigarettes.

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PUM

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Abstract

The invention provides a preparation method of a grape juice Maillard cigarette flavor. An ammonia substance is added to grape juice, the mixture is placed into a reaction kettle after stirred and is stirred into a uniform reaction system, the pH value of the reaction system is adjusted by an acid or alkali compound, then a return pipe is mounted, the reaction system is heated while stirring to have a Maillard reaction under the normal pressure, and the tobacco flavor is prepared. The tobacco flavor has the strong brunt and sweet fragrance, can improve cigarette sweetness and fragrance and promote smoke emission, is lively and can significantly improve the cigarette quality.

Description

Technical field [0001] The invention relates to a method for preparing flavors for tobacco, in particular to a method for preparing flavors for grape juice Maillard tobacco. technical background [0002] At present, the tobacco flavors used in cigarettes in my country generally adopt two major categories: one is natural extract flavors, which use natural components contained in natural flavors or potentially coordinated with smoke; the other is synthetic flavors, which use synthetic It is a fragrance monomer that is coordinated with smoke and has a certain effect on smoke. Tobacco flavors made by these two types of flavors alone or formulated, although the process is simple, but due to the monotonous flavor, single effect on smoke, the effect is not very good. my country's research on tobacco flavors has been relatively backward, and most flavors depend on imports. Therefore, it is necessary to develop effective tobacco flavors. [0003] Some people in China simply react glucose w...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24B15/28
Inventor 张敦铁庞登红尹团章王萍周湘
Owner HUBEI CHINA TOBACCO IND
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