Method for preparing zirconia aerogel by secondary gel method combined with atmospheric drying
An atmospheric drying and aerogel technology, applied in zirconia and other directions, can solve the problems of expensive equipment, difficult mass production, and high cost, and achieve the effect of improving the strength of the skeleton
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specific Embodiment approach 1
[0025] Specific embodiment one: In this embodiment, the method for preparing zirconia airgel by secondary gel method combined with normal pressure drying is carried out according to the following steps:
[0026] 1. Preparation of zirconia wet gel
[0027] Under stirring conditions, the ZrO(NO 3 ) 2 2H 2 Dissolve O in an alcoholic water solvent to make a transparent solution with a zirconyl nitrate concentration of 4.9-5.1wt%, then add formamide dropwise to the solution to obtain a mixed solution, and put the mixed solution in a water bath at a temperature of 60°C In a water bath, add ammonia water drop by drop to adjust the pH of the mixture to 8.7-9.3, then increase the stirring rate, stop stirring after 5-8 minutes, the gel is in a thick soup state, and continue to bathe at 60°C;
[0028] 2. ZrO 2 Regelation and Modification of Thick Gel
[0029] Transfer the thick soup-like gel prepared in step 1 to an oven at 43-47°C for aging until a wet gel solid is formed for the s...
specific Embodiment approach 2
[0032] Embodiment 2: The difference between this embodiment and Embodiment 1 is that in Step 1, a transparent solution with a zirconyl nitrate concentration of 5 wt % is prepared. Others are the same as in the first embodiment.
specific Embodiment approach 3
[0033] Embodiment 3: The difference between this embodiment and Embodiment 1 or 2 is that the alcohol-water solvent in step 1 is made of absolute ethanol and water at a volume ratio of 2.8 to 3.2:1. Others are the same as in the first or second embodiment.
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