High-temperature-resistant salt-tolerant filtrate loss reducer and preparation method thereof

A fluid loss reducing agent, high temperature resistant technology, applied in the field of oil resource exploration and development, can solve problems such as wellbore instability, achieve the effect of reducing fluid loss, excellent fluid loss reduction performance, and solving wellbore instability

Inactive Publication Date: 2016-07-06
BC P INC CHINA NAT PETROLEUM CORP +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] In order to solve the above-mentioned technical problems, the object of the present invention is to provide a high-temperature-resistant, salt-resistant fluid loss reducer, which can effectively reduce the fluid loss of the high-temperature saturated brine-based drilling fluid system and maintain the performance of the drilling fluid system It solves the problem of well wall instability caused by excessive drilling fluid filtration loss during drilling high temperature and high salt deep wells

Method used

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  • High-temperature-resistant salt-tolerant filtrate loss reducer and preparation method thereof
  • High-temperature-resistant salt-tolerant filtrate loss reducer and preparation method thereof
  • High-temperature-resistant salt-tolerant filtrate loss reducer and preparation method thereof

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Embodiment 1

[0029] This embodiment provides a high temperature resistant, salt tolerant fluid loss control agent, the preparation method of the fluid loss control agent comprises the following steps:

[0030] 1) Add 220 parts of pure water into a four-necked flask, and add 7.5 parts of acrylamide, 21 parts of 2-acrylamide-2-methylpropanesulfonic acid, 25 parts of sodium styrene sulfonate and 3.5 parts of horse to anhydride, stirred until dissolved;

[0031] 2) Add 34.58 parts of sodium hydroxide aqueous solution to the above-mentioned four-necked flask to adjust the pH value to 7.0, then add 5 parts of 2% (mass percentage concentration) ammonium persulfate aqueous solution, and continue stirring;

[0032] 3) Heat the four-neck flask to 80°C, and react at this temperature for 1-3 hours at a constant temperature, and obtain a fluid loss control agent solution after the reaction;

[0033] 4) Vacuum-dry the fluid loss control agent solution at 35° C., and then crush and sieve it (through a 2...

Embodiment 2

[0035] This embodiment provides a high temperature resistant, salt tolerant fluid loss control agent, the preparation method of the fluid loss control agent comprises the following steps:

[0036] 1) Add 220 parts of pure water into a four-necked flask, and add 5 parts of acrylamide, 15 parts of 2-acrylamide-2-methylpropanesulfonic acid, 20 parts of sodium styrene sulfonate and 5 parts of horse to anhydride, stirred until dissolved;

[0037] 2) Add 34.9 parts of sodium hydroxide aqueous solution to the above-mentioned four-necked flask to adjust the pH value to 7.0, then add 4 parts of 2% ammonium persulfate aqueous solution, and stir;

[0038] 3) Heat the four-necked flask to 80°C, and react at this temperature for 1-3 hours at a constant temperature, and obtain a fluid loss control agent solution after the reaction is completed;

[0039] 4) Vacuum-dry the fluid loss control agent solution at 35° C., and then crush and sieve it (through a 200-mesh sieve) to obtain the finish...

Embodiment 3

[0041] This embodiment provides a high temperature resistant, salt tolerant fluid loss control agent, the preparation method of the fluid loss control agent comprises the following steps:

[0042] 1) Add 220 parts of pure water into a four-necked flask, and add 10 parts of acrylamide, 25 parts of 2-acrylamide-2-methylpropanesulfonic acid, 30 parts of sodium styrene sulfonate and 4 parts of horse to anhydride, stirred until dissolved;

[0043] 2) Add 40.48 parts of aqueous sodium hydroxide solution to the above-mentioned four-necked flask to adjust the pH value to 7.0, then add 6 parts of 2% aqueous ammonium persulfate solution, and stir;

[0044] 3) Heat the four-necked flask to 80°C, and react at this temperature for 1-3 hours at a constant temperature, and obtain a fluid loss control agent solution after the reaction is completed;

[0045] 4) Vacuum-dry the fluid loss control agent solution at 35° C., and then crush and sieve it (through a 200-mesh sieve) to obtain the fini...

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Abstract

The invention provides a high-temperature-resistant salt-tolerant filtrate loss reducer and a preparation method thereof.The high-temperature-resistant salt-tolerant filtrate loss reducer comprises, by weight, 3-10 parts of acrylamide, 15-25 parts of 2-acrylamido-2-methylpropane sulfonic acid, 20-40 parts of sodium p-styrene sulfonate, 3-8 parts of maleic anhydride, 27-52 parts of aqueous sodium hydroxide, 3-6 parts of aqueous ammonium persulfate and 220 parts of purified water.The preparation method of the high-temperature-resistant salt-tolerant filtrate loss reducer includes adding the purified water, the acrylamide, the 2-acrylamido-2-methylpropane sulfonic acid, the sodium p-styrene sulfonate and the maleic anhydride into a container prior to dissolving, and adding the aqueous sodium hydroxide and the aqueous ammonium persulfate to undergo thermostatic reaction so as to obtain the filtrate loss reducer.The high-temperature-resistant salt-tolerant filtrate loss reducer is capable of decreasing filtrate loss quantity of a high-temperature saturated saltwater-based drilling fluid system to keep the drilling fluid system stable in performance, so that the problems of wellbore instability caused by large filtrate loss quantity of a wellbore in a high-temperature high-salinity bore drilling process and the like are solved.

Description

technical field [0001] The invention relates to a high-temperature-resistant and salt-resistant fluid loss reducer, which belongs to the technical field of oil resource exploration and development. Background technique [0002] With the continuous deepening of oil exploration and development in my country, the exploration and development of deep oil and natural gas has gradually become the main way to solve the problem of stable and increased production in my country's oil industry. Therefore, the drilling of deep wells and ultra-deep wells will definitely become an important aspect of my country's oil industry. [0003] The deeper the wellbore, the higher the temperature inside the wellbore due to the existence of the geothermal gradient. In the western oilfields (temperature gradient of 2.5-3.0℃ / 100m) of ultra-deep wells exceeding 7000m and in the eastern oilfields (temperature gradient of 3.5-4.3℃ / 100m) of deep wells exceeding 5000m, the bottom hole temperature is likely ...

Claims

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Application Information

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IPC IPC(8): C09K8/03C09K8/16C09K8/18
CPCC09K8/03C09K8/16C09K8/18
Inventor王茂功杨泽星陈帅
OwnerBC P INC CHINA NAT PETROLEUM CORP