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129 results about "2-Acrylamido-2-methylpropane sulfonic acid" patented technology

2-Acrylamido-2-methylpropane sulfonic acid (AMPS) was a Trademark name by The Lubrizol Corporation. It is a reactive, hydrophilic, sulfonic acid acrylic monomer used to alter the chemical properties of wide variety of anionic polymers. In the 1970s, the earliest patents using this monomer were filed for acrylic fiber manufacturing. Today, there are over several thousands patents and publications involving use of AMPS in many areas including water treatment, oil field, construction chemicals, hydrogels for medical applications, personal care products, emulsion coatings, adhesives, and rheology modifiers.

Vinyl alcohol copolymers for use in aqueous dispersions and melt extruded articles

In a method of preparing an aqueous dispersion selected from drilling fluids, hydraulic cement compositions, mineral pigment containing coatings, and papermaking furnishes or in a method of preparing a melt extrudate, the improvement comprising: a) producing a copolymer of vinyl alcohol (VOH) and 2-acrylamido-2-methyl propane sulfonic acid or a salt of such acid (AMPS) by steps including continuously feeding with agitation, vinyl acetate (VAM) and AMPS as comonomers, a free radical yielding polymerization initiator, and a solvent for said comonomers, initiator, and copolymer resulting from the copolymerization of said comonomers, maintaining the resulting reaction mass in said first reaction zone under polymerization conditions for a residence time sufficient for a major proportion of AMPS fed to said first reaction zone to polymerize, continuously feeding reaction mass from said first reaction zone with an additional supply of AMPS to a second reaction zone, maintaining the reaction mass in the second reaction zone for a residence time sufficient to polymerize a major proportion of the AMPS added to the second reaction zone, continuously withdrawing reaction mass from the second reaction zone, separating copolymer of VAM and AMPS from the latter reaction mass, and saponifying by hydrolysis and/or alcoholysis a major proportion of the acetate groups in said copolymer to form a copolymer of VOH and AMPS; and b) incorporating the saponified copolymer into the aqueous dispersion or melt extrudate.
Owner:SEKISUI SPECIALTY CHEM AMERICA

Vinyl alcohol copolymers for use in aqueous dispersions and melt extruded articles

In a method of preparing an aqueous dispersion selected from drilling fluids, hydraulic cement compositions, mineral pigment containing coatings, and papermaking furnishes or in a method of preparing a melt extrudate, the improvement comprising:a) producing a copolymer of vinyl alcohol (VOH) and 2-acrylamido-2-methyl propane sulfonic acid or a salt of such acid (AMPS) by steps including continuously feeding with agitation, vinyl acetate (VAM) and AMPS as comonomers, a free radical yielding polymerization initiator, and a solvent for said comonomers, initiator, and copolymer resulting from the copolymerization of said comonomers, maintaining the resulting reaction mass in said first reaction zone under polymerization conditions for a residence time sufficient for a major proportion of AMPS fed to said first reaction zone to polymerize, continuously feeding reaction mass from said first reaction zone with an additional supply of AMPS to a second reaction zone, maintaining the reaction mass in the second reaction zone for a residence time sufficient to polymerize a major proportion of the AMPS added to the second reaction zone, continuously withdrawing reaction mass from the second reaction zone, separating copolymer of VAM and AMPS from the latter reaction mass, and saponifying by hydrolysis and / or alcoholysis a major proportion of the acetate groups in said copolymer to form a copolymer of VOH and AMPS; andb) incorporating the saponified copolymer into the aqueous dispersion or melt extrudate.
Owner:SEKISUI SPECIALTY CHEM AMERICA

Anti-pollution separation membrane and preparation method

The invention discloses an anti-pollution separation membrane and a preparation method, wherein aiming at the shortages of a preparation technology for the present anti-pollution PVDF (polyvinylidene fluoride) separation membrane, the invention provides a novel method for preparing an anti-microbial pollution PVDF separation membrane. The novel method provided by the invention comprises the following steps of: synthesising the random copolymer with a zwitterionic structure, of MMA (methl methacrylate), DMC (dimethyl carbonate) and AMPS (2-acrylamido-2-methylpropane sulfonic acid) via free radical polymerization at first, adding the copolymer and a porogenic agent, i.e., polyethylene glycol (PEG) in PVDF, and preparing the anti-pollution separation membrane by using N,N-dimethyl formamide (DMF) as a solvent and using water as a coagulating agent through a phase inversion method. Electropositive quaternary amine group and electronegative sulfonic group exist in the structure of the copolymer simultaneously, and have a binding capacity for water molecules which is much stronger than the binding capacity of traditional polyethylene glycol and the derivatives of the traditional polyethylene glycol, and the formed hydration layer is more stable; therefore, the prepared novel PVDF membrane is lasting in anti-pollution performance.
Owner:TIANJIN POLYTECHNIC UNIV

Acrylamide/2-acrylamido-2-methylpropane sulfonic acid sodium/cyclodextrin modified acrylamide (AM/AMPS-Na/MAM) copolymer and preparation method thereof

The invention discloses acrylamide / 2-acrylamido-2-methylpropane sulfonic acid sodium / cyclodextrin modified acrylamide (AM / AMPS-Na / MAM) copolymer serving as a fluid loss reducer for drilling fluid in oilfield, and a preparation method thereof, which can solve the problems of short cement paste thickening time, failure of an additive and high filter loss due to strata pressure and temperature rise. The technical scheme is that: the copolymer is prepared by polymerizing 83 to 85 percent of acrylamide AM, 15 to 16 percent of 2-acrylamido-2-methylpropane sulfonic acid sodium AMPS-Na and 1 to 2 percent of cyclodextrin modified acrylamide MAM. The preparation method comprises the following steps of: adding aqueous solution of the AM, solution of the MAM and solution of the AMPS-Na into a reaction container; adding ethylene diamine tetraacetic acid, potassium peroxydisulfate and sodium hydrogensulfite; and stirring uniformly, and reacting at the temperature of between 40 and 50DEG C for 5 to 6 hours under the protection of nitrogen to obtain the AM / AMPS-Na / MAM copolymer. The AM / AMPS-Na / MAM copolymer serving as a drilling fluid treating agent has high thermal stability, high temperature resistance, and better fluid loss reducing effect; the preparation method is simple and practicable, and the reaction conditions are mild; and the AM / AMPS-Na / MAM copolymer is used as the drilling fluid treating agent in the oilfield.
Owner:SOUTHWEST PETROLEUM UNIV

Double electron type polymerizable surfactant monomer, and preparation method and applications thereof

The invention discloses a double electron type polymerizable surfactant monomer. A preparation method comprises following steps: 1, epoxy chloropropane and a long chain tertiary amine are subjected toring-opening reaction in a hydrochloric acid solution so as to obtain an intermediate EPT; 2, EPT and N-dimethyl aminopropyl methacrylamide are subjected to quaterisation so as to obtain a finial product. The double electron type polymerizable surfactant monomer, acrylamide, acrylic acid, and 2-acrylamido-2-methylpropane sulfonic acid are subjected to polymerization, drying, crushing, and sievingat room temperature so as to obtain a polymer thickening agent powder; the polymer thickening agent powder is prepared into a 0.3wt% solution which is taken as a fracturing fluid. The preparation method is friendly to the environment; cost is low; yield and purity are relatively high; the hydrophobic associated polymer solution based on the monomer possesses excellent viscoelasticity and temperature resistance and salt resistance, so that the fracturing liquid prepared from the monomer is capable of solving technical problems in the prior art that conventional hydrophobic associated polymer fracturing liquid cost is high, and sand suspension capacity is poor.
Owner:SOUTHWEST PETROLEUM UNIV

High-temperature-resistant slow-release scale inhibitor

The invention relates to the field of water treatment chemicals, in particular to a high-temperature-resistant slow-release scale inhibitor. The high-temperature-resistant slow-release scale inhibitor comprises the following substances in parts by weight: 6-12 parts of a starch substrate, 12-15 parts of acrylic acid, 6-10 parts of 2-acrylamido-2-methylpropane sulfonic acid, 20-25 parts of polyaspartic acid, 5-10 parts of a nitrogen-containing heterocyclic compound composition, 10-15 parts of water-soluble oxidative inorganic metal salt, 5-10 parts of water-soluble inorganic zinc salt, 5-10 parts of homopolycarboxylic acid, 5-10 parts of lignosulfonate, 10-15 parts of sodium polyhydroxy carboxylate, 5-10 parts of a cellulose derivative, 5-8 parts of a composite initiator, 3-6 parts of a dispersed activator and 5-10 parts of an auxiliary corrosion inhibitor. The high-temperature-resistant slow-release scale inhibitor provided by the invention is low in cost, wide in source, friendly to environment, nontoxic and free from secondary pollution; the scale inhibitor is resistant to high temperature, can effectively inhibit the formation of calcium carbonate scales, calcium sulfate scales, barium sulfate scales and calcium phosphate scales in an oilfield pipeline and a boiler, has a good slow release effect on the pipeline and the boiler, and can prolong the service life.
Owner:QINGDAO HUANAN SHENGYUAN FRUIT IND CO LTD
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