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A kind of organic deicing agent and preparation method thereof

A snow-melting agent and organic technology, applied in the field of applied chemistry, can solve the problems of large corrosion and damage of chloride salts, high production cost, environmental pollution, etc., and achieve the effects of saving resources, small corrosion and damage, and protecting the environment.

Active Publication Date: 2017-09-12
辽宁省交通科学研究院有限责任公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Aiming at the problems of high production cost of non-chloride salt deicing agent calcium magnesium acetate CMA, narrow application range of snow melting and deicing temperature, large corrosion damage of chlorine salts, and serious environmental pollution in the prior art, the present invention proposes an organic deicing agent and its preparation method

Method used

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  • A kind of organic deicing agent and preparation method thereof
  • A kind of organic deicing agent and preparation method thereof
  • A kind of organic deicing agent and preparation method thereof

Examples

Experimental program
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Effect test

Embodiment 1

[0050]An organic deicing agent, the composition is by mass percentage: 8% calcium succinate, 22% magnesium succinate, 14% calcium glutarate, 38% magnesium glutarate, 5% calcium adipate %, magnesium adipate is 13%.

[0051] A kind of preparation method of organic deicing agent, comprises the following steps:

[0052] Step 1, weighing 100g of mixed dibasic acid, mixed with 300g of distilled water, to prepare a mixed dibasic acid aqueous solution with a mass concentration of 25%;

[0053] Step 2, calculate and take by weighing the actual dosage of salinization reagent; Wherein, the composition of salinization reagent, by the percentage of the amount of substance, dolomite powder n 1 : Magnesium carbonate powder n 2 = 50%: 50%;

[0054] (1) Calculate the actual dosage W of the salinizing reagent, and calculate according to the formula (I), (II), and (III):

[0055] As can be seen from formula (I), acid value=600 (mg NaOH / g);

[0056] It can be seen from the formula (II) that ...

Embodiment 2

[0072] An organic deicing agent, the composition is by mass percentage: 10% of calcium succinate, 19.5% of magnesium succinate, 18.5% of calcium glutarate, 33.5% of magnesium glutarate, 6.5% of calcium adipate %, magnesium adipate is 12%.

[0073] A kind of preparation method of organic deicing agent, comprises the following steps:

[0074] Step 1, weigh 100g of mixed dibasic acid, mix it with 400g of distilled water, and prepare an aqueous solution of mixed dibasic acid with a mass concentration of 20%;

[0075] Step 2, calculate and take by weighing the actual dosage of salinization reagent; Wherein, the composition of salinization reagent, by the percentage of the amount of substance, dolomite powder n 1 : Magnesium carbonate powder n 2 = 66.7%: 33.3%;

[0076] (1) Calculate the actual dosage W of the salinizing reagent, and calculate according to the formula (I), (II), and (III):

[0077] As can be seen from formula (I), acid value=600 (mg NaOH / g);

[0078] It can be ...

Embodiment 3

[0092] An organic deicing agent, the composition is by mass percentage: 1.5% of calcium succinate, 27% of magnesium succinate, 3% of calcium glutarate, 49.5% of magnesium glutarate, 1% of calcium adipate %, magnesium adipate is 18%.

[0093] A kind of preparation method of organic deicing agent, comprises the following steps:

[0094] Step 1, weigh 100g of mixed dibasic acid, mix it with 350g of distilled water, and prepare a mixed dibasic acid aqueous solution with a mass concentration of 22.2%;

[0095] Step 2, calculate and take by weighing the actual dosage of salinization reagent; Wherein, the composition of salinization reagent, by the percentage of the amount of substance, dolomite powder n 1 : Magnesium carbonate powder n 2 = 10%: 90%;

[0096] (1) Calculate the actual dosage W of the salinizing reagent, and calculate according to the formula (I), (II), and (III):

[0097] As can be seen from formula (I), acid value=600 (mg NaOH / g);

[0098] It can be seen from th...

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Abstract

The invention discloses an organic snow-melting agent and a preparation method thereof and belongs to the technical field of applied chemistry.The organic snow-melting agent is prepared from, by mass, 1.5-15% of calcium succinate, 15-30% of magnesium succinate, 3-25% of calcium glutarate, 25-50% of magnesium glutarate, 1-10% of calcium adipate and 10-20% of magnesium adipate.The preparation method of the organic snow-melting agent comprises the following steps of 1, preparing a mixed diacid aqueous solution; 2, calculating and weighing the actual adding volume of salinization reagent; 3, conducting mixing; 4, conducting filtering; 5, conducting decolouration treatment; 6, conducting evaporation for separation.The prepared novel non-chlorine-salt type organic snow-melting agent is mixed with diacid calcium and magnesium and is applicable to snow melting and deicing of places with the temperature being 15 DEG C or above, compared with snow-melting agents of the same type, namely calcium acetate and magnesium acetate, which are commonly used on the market, the applicable temperature range is broadened by about 5 DEG C, and the corrosion damage effect is extremely small; a new path is opened up for recycling of a byproduct, namely mixed diacid, in the nylon production industry, resources are saved, and the environment is protected.

Description

technical field [0001] The invention belongs to the technical field of applied chemistry, and in particular relates to an organic deicing agent and a preparation method thereof. Background technique [0002] Deicing agent is a kind of chemical substance that can make ice and snow melt into liquid below 0 ℃, there are solid and liquid. The deicing agent achieves the purpose of melting snow and ice by lowering the freezing point of water so that the water does not condense into a solid state within a certain temperature range below zero. It is used for snow removal in winter on roads, airports, railways, squares and other places, reducing the slippery road surface and improving the safety of vehicles driving on the road surface. Safety, to ensure the smooth flow of traffic and the safety of people's lives and property. In the 1950s, Europe and the United States first started to use deicing agents. At present, the most widely used deicing agents at home and abroad are chlorine...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09K3/18
CPCC09K3/185
Inventor 吴玉辉刘云金范兴华朱建平高明
Owner 辽宁省交通科学研究院有限责任公司
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