Production process of Xinjiang brown cattle cholic acid

A production process, cholic acid technology, applied in the field of livestock breeding, can solve problems such as complex process and low production efficiency, achieve broad market prospects, low production cost, and reduce production processes

Inactive Publication Date: 2016-11-09
LIUZHOU CITY LIUNAN DISTRICT ANSHUN BREEDING ASSOCS
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The existing production process of bovine and sheep cholic acid has complicated process and low production efficiency

Method used

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Embodiment Construction

[0011] The technical solution of the present invention will be described in detail below.

[0012] In order to solve the above-mentioned problems existing in prior art and actual situation, the invention provides a kind of production technology of Xinjiang brown taurocholic acid, it is characterized in that, comprises the following steps:

[0013] 1) Collect the bitter gall of fresh Xinjiang brown cattle, cut the gall skin, collect the bile and filter it, stir well, add 0.1 times (10%) to the total weight of the bile, add sodium hydroxide (caustic soda, caustic soda) and stir to boil , 24 hours of silk melting, add water at any time during the silk melting;

[0014] 2) After the silk is melted, cool to room temperature, siphon the upper clear night, filter the lower precipitate with a cloth (combined filtrate) into another container, cool to below room temperature, then add 2-3% hydrogen peroxide and stir for 15 minutes, stand still Precipitate for 30 minutes;

[0015] 3) ad...

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PUM

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Abstract

The invention provides a production process of Xinjiang brown cattle cholic acid. The production process comprises the following steps: shearing gall skin, collecting bile and filtering, evenly stirring, adding 0.1 times of the total weight of bile, adding sodium hydroxide, stirring and heating to boil, saponifying for 24h, supplementing clean water during saponification, after completion of saponification, cooling to room temperature, collecting a supernatant by a siphon, filtering a lower precipitate with a cloth filter to another container, cooled to below room temperature, and then adding 2 to 3% hydrogen peroxide (H2O2), fully stirring for 15min, keeping stand and precipitating for 30min; filtering by adding acid, stirring, and precipitating; after the cholic acid floats out of a liquid surface, fishing out a floater, putting in a pot, adding 2 times of the amount of clean water and ethyl acetate, evenly stirring, heating to boil for 30 minutes, forming cholic acid particles, filtering, washing with clean water to be neutral, and hanging to dry to obtain a semi-finished product of Xinjiang brown cattle cholic acid; introducing an alcohol and hydrogen peroxide mixture according to a ratio of 100: 2-3 into the semi-finished product of Xinjiang brown cattle cholic acid, stirring to a mixed feed shape, and spin-drying with a centrifuge.

Description

technical field [0001] The invention relates to the technical field of livestock breeding, in particular to a production process of Xinjiang brown taurocholic acid. Background technique [0002] In recent years, my country's animal husbandry has continued to develop at a high speed. Among cattle and sheep animals, bile acid exists in the bile of many vertebrates, and the bile of cattle, sheep and dogs is the most abundant, and it is used as a raw material for the preparation of artificial bezoar. The existing production technology of bovine and sheep cholic acid has complicated technology and low production efficiency. Contents of the invention [0003] In order to solve the above-mentioned problems existing in prior art and actual situation, the invention provides a kind of production technology of Xinjiang brown taurocholic acid, it is characterized in that, comprises the following steps: [0004] 1) Collect the bitter gall of fresh Xinjiang brown cattle, cut the gall s...

Claims

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Application Information

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IPC IPC(8): C07J9/00
CPCC07J9/005
Inventor何以安
OwnerLIUZHOU CITY LIUNAN DISTRICT ANSHUN BREEDING ASSOCS