Method for improving extraction rate of volatile oil of rhizoma acori graminei by re-extraction
A technology of volatile oil and calamus, applied in the field of volatile oil extraction, can solve the problems of long time, high temperature, complicated process, etc., and achieve the effect of increasing utilization rate, small component damage, and high purification rate
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[0035] (1) Take 70g of Shichangpu medicinal material, put it in a 1000ml round bottom flask, add 560ml of water, soak for 4h, extract respectively: 4h, 5h, 6h, 7h, 8h..., compare the volume of extracted Shichangpu volatile oil, as figure 1 As shown, when the extraction time is 6h, the volume of the initial extraction of the volatile oil of Shichangpu is constant, and the constant time of the initial extraction volume of the volatile oil of Shichangpu is determined to be 6h.
[0036] (2) Under the same conditions, take 70g of Acorus calamus again, put it in a 1000ml round bottom flask, add 560ml of water, soak for 4 hours, and initially extract for 6 hours. Carry out re-extraction, respectively at intervals of 2h, 4h, 8h, 12h, extract for 5h, and compare the volume of the volatile oil of Acorus calamus, as figure 2 As shown, when the interval time is 4h, the re-extraction volume of Shichangpu is the largest, so the interval time between re-extraction is determined to be 4h.
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