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Tobacco curing-flavor filter capable of reducing heavy metal content in flue gas and preparation method thereof

A heavy metal and filter technology, which is applied in the fields of tobacco, e-liquid filter elements, applications, etc., can solve the problems of increasing the irritation and miscellaneous gas of cigarettes, and the unobtrusive aroma of roasted aroma, so as to improve the quality of roasted aroma and reduce the cost , The effect of reducing the content of heavy metals

Active Publication Date: 2021-08-03
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, the roasted fragrance of the above-mentioned products obtained is not outstanding, and still contains a certain amount of macromolecular substances such as protein, pectin, and polysaccharides, which will be cracked to produce some harmful components during the smoking process of cigarettes, which will increase the quality of cigarettes. Suction irritation and fumes

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0033] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:

[0034] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 150°C for 3 hours in a container connected with a condensation reflux device;

[0035] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;

[0036] Described polyhydric alcohol is ethylene glycol;

[0037] The organic acid-metal salt compound is a ferric chloride-ethylenediaminetetraacetic acid compound (molar ratio 1:3);

[0038] In step (2), add the product obtained in step (1) into an organic solvent, perform ultrasonic extraction for 60 minutes, then shake and extract for 60 minutes, then centrifuge for 15 minutes, take the upper liquid and filter it with an organic filter membrane, and then take the filtrate and distill it under reduced pressure. That is, the conc...

Embodiment 2

[0051] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:

[0052] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 250°C for 0.5h in a container connected with a condensation reflux device;

[0053] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;

[0054] The polyols are ethylene glycol and propylene glycol (mass ratio is 1:1);

[0055] The organic acid-metal salt compound is zinc lactate-tartaric acid compound (molar ratio 1:5);

[0056] Step (2), adding the product obtained in step (1) into an organic solvent, ultrasonically extracting for 10-60 minutes, then shaking and extracting for 10-60 minutes, and then centrifuging for 4-15 minutes, taking the upper liquid and filtering it with an organic filter membrane, The filtrate was distilled under reduced pressure to obtain the ...

Embodiment 3

[0067] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:

[0068] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 200°C for 1 hour in a container connected with a condensation reflux device;

[0069] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;

[0070] The polyhydric alcohol is one or a combination of glycerin;

[0071] The organic acid-metal salt compound is zinc lactate-tartaric acid compound (molar ratio 1:5);

[0072] In step (2), add the product obtained in step (1) into an organic solvent, perform ultrasonic extraction for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 10 minutes, take the upper liquid and filter it with an organic filter membrane, then take the filtrate and distill it under reduced pressure, That is, the concentrate is obtain...

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PUM

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Abstract

The invention relates to a tobacco-cured flavor filter tip capable of reducing the content of heavy metals in smoke and a preparation method thereof, which belongs to the technical field of tobacco auxiliary materials. The method is to add polyhydric alcohol and organic acid-metal salt compound to tobacco powder, after mixing, heat in a container connected with a condensing reflux device for reaction; add the obtained product into an organic solvent, and first ultrasonically extract, Then shake and extract, then centrifuge, take the upper liquid and filter it with an organic filter, distill the filtrate under reduced pressure, prepare the obtained concentrate into a solution with a mass concentration of 1% to 5%, and add polyferric sulfate to the solution to mix Homogenize and then alcoholize, and finally add the alcoholized liquid evenly to the filter tow, and make the filter according to the conventional method, that is, obtain the tobacco roasted flavor filter. The preparation method of the invention is simple, the cost is low, and the prepared filter tip can significantly reduce the heavy metal content of cigarette smoke, and can reduce the amount of miscellaneous gas and has good application prospect.

Description

technical field [0001] The invention belongs to the technical field of tobacco auxiliary materials, and in particular relates to a tobacco roasting flavor filter tip capable of reducing the content of heavy metals in smoke and a preparation method thereof. Background technique [0002] As cigarette consumers pay more and more attention to their own health and have higher and higher requirements on the intrinsic quality of cigarettes, low-tar and high-quality cigarettes have become the focus of current research. However, low tar must be accompanied by loss of cigarette aroma and poor comfort. In terms of quality, the current domestic cigarette products have certain deficiencies in smoking quality and sensory comfort, such as weak aroma, strong dryness, insufficient sweetness, and poor comfort. [0003] At present, directly adding some flavoring substances with flavoring and sweetening effects into the filter rod has become a very potential compensation application method. T...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): A24D3/02A24D3/04
CPCA24D3/022A24D3/048
Inventor 向明张承明王晋刘强张建荣张涛耿永勤蒋次清魏玉玲田丽梅陈章玉
Owner CHINA TOBACCO YUNNAN IND