Tobacco curing-flavor filter capable of reducing heavy metal content in flue gas and preparation method thereof
A heavy metal and filter technology, which is applied in the fields of tobacco, e-liquid filter elements, applications, etc., can solve the problems of increasing the irritation and miscellaneous gas of cigarettes, and the unobtrusive aroma of roasted aroma, so as to improve the quality of roasted aroma and reduce the cost , The effect of reducing the content of heavy metals
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Embodiment 1
[0033] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:
[0034] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 150°C for 3 hours in a container connected with a condensation reflux device;
[0035] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;
[0036] Described polyhydric alcohol is ethylene glycol;
[0037] The organic acid-metal salt compound is a ferric chloride-ethylenediaminetetraacetic acid compound (molar ratio 1:3);
[0038] In step (2), add the product obtained in step (1) into an organic solvent, perform ultrasonic extraction for 60 minutes, then shake and extract for 60 minutes, then centrifuge for 15 minutes, take the upper liquid and filter it with an organic filter membrane, and then take the filtrate and distill it under reduced pressure. That is, the conc...
Embodiment 2
[0051] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:
[0052] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 250°C for 0.5h in a container connected with a condensation reflux device;
[0053] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;
[0054] The polyols are ethylene glycol and propylene glycol (mass ratio is 1:1);
[0055] The organic acid-metal salt compound is zinc lactate-tartaric acid compound (molar ratio 1:5);
[0056] Step (2), adding the product obtained in step (1) into an organic solvent, ultrasonically extracting for 10-60 minutes, then shaking and extracting for 10-60 minutes, and then centrifuging for 4-15 minutes, taking the upper liquid and filtering it with an organic filter membrane, The filtrate was distilled under reduced pressure to obtain the ...
Embodiment 3
[0067] A method for preparing a tobacco-cured aroma filter capable of reducing the content of heavy metals in flue gas, comprising the following steps:
[0068] Step (1): Add polyol and organic acid-metal salt compound to tobacco powder, mix well, and react at 200°C for 1 hour in a container connected with a condensation reflux device;
[0069] The tobacco powder is a combination of flue-cured tobacco, oriental tobacco and sun-cured red tobacco;
[0070] The polyhydric alcohol is one or a combination of glycerin;
[0071] The organic acid-metal salt compound is zinc lactate-tartaric acid compound (molar ratio 1:5);
[0072] In step (2), add the product obtained in step (1) into an organic solvent, perform ultrasonic extraction for 30 minutes, then shake and extract for 30 minutes, then centrifuge for 10 minutes, take the upper liquid and filter it with an organic filter membrane, then take the filtrate and distill it under reduced pressure, That is, the concentrate is obtain...
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