Method for determining wax contents in asphalt

A determination method and technology for wax content, applied in the measurement of color/spectral characteristics, etc., can solve the problems of unsuitable asphalt production process quality control analysis, rapid detection of unfavorable asphalt samples, poor repeatability and reproducibility, etc., and achieve test and analysis results. Reliable, simple test method, good repeatability and reproducibility

Inactive Publication Date: 2019-02-22
LUOYANG INST OF SCI & TECH
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Problems solved by technology

The existing standard uses the cracking method to detect the wax content of asphalt. The method is cumbersome, the operation is complicated, and a large amount of toxic solvents are used, which consumes a long time. At the same time, there are human factors in the measurement process, and the repeatability and reproducibility are poor. Therefore, It is not conducive to the rapid detection of asphalt samples, and it is not suitable for quality control analysis in the asphalt production process and road construction process. Therefore, it is of great practical significance to study an accurate, fast, pollution-free and easy-to-operate asphalt detection method

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  • Method for determining wax contents in asphalt
  • Method for determining wax contents in asphalt
  • Method for determining wax contents in asphalt

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Embodiment Construction

[0051] The following will clearly and completely describe the technical solutions in the embodiments of the present invention with reference to the drawings in the embodiments of the present invention.

[0052] A kind of assay method of wax content in asphalt, operation steps are as follows:

[0053] 1. First, prepare road asphalt samples of different oil sources, production processes, brands, models, and batches, and test the wax content according to the current test method.

[0054] 2. Prepare the infrared disc detection sample, use the silica gel test mold with the same aperture and thickness to ensure the equal quality, equal thickness and equal area of ​​the asphalt sample, and the size of the silica gel test mold is consistent with the area and thickness of the infrared spectrometer sample platform ; The test mold for preparing the sample is a silica gel test mold, which does not stick to the asphalt, and the asphalt can be quickly formed in the test mold and can be quic...

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Abstract

The invention relates to a method for determining wax contents in asphalt, and belongs to the field of road engineering asphalt quality detection. The method comprises the steps of: preparing a sample, collecting an infrared spectrum of the sample by using an infrared spectrometer, and obtaining an average spectrum figure through an ATR manner; selecting an appropriate spectral segment as a modeling interval, carrying out baseline correction processing and peak processing on the spectrum by utilizing relevant software, and carrying out regression or fitting analysis on data of the modeling interval by using a mathematic method so as to establish a regression model; and predicting wax content in the unknown sample by utilizing the model. The method is low in error rate and is capable of carrying out real-time, in-situ, non-destructive, rapid and quantitative analysis on asphalt wax contents.

Description

technical field [0001] The invention belongs to the field of road engineering asphalt quality detection, and in particular relates to a method for measuring wax content in asphalt. Background technique [0002] Asphalt pavement is widely used in our country because of its excellent road performance and good service performance. As a binder to improve the performance of asphalt pavement, more and more attention has been paid to the performance of asphalt during use, among which wax content, softening point and penetration are the most important. On the one hand, it is because the wax is dispersed in the asphalt after crystallization and precipitation in a low-temperature environment, which reduces the compactness between the asphalt molecules and significantly reduces the low-temperature ductility of the asphalt; Decrease, increase sensitivity to asphalt. Wax can also reduce the adhesion between asphalt and the stone surface, and in the presence of water, it is easy to caus...

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N21/35
CPCG01N21/35
Inventor 王丽王志祥
Owner LUOYANG INST OF SCI & TECH
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