Preparation and application of a magnetic one-dimensional chain nanocomposite
A nanocomposite and chain-like technology, applied in the field of nanomaterials, can solve problems such as application limitations, unstable performance of magnetic one-dimensional nanomaterials, and complicated preparation process, and achieve the effects of simple and easy operation, prevention of agglomeration, and avoidance of corrosion
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Embodiment 1
[0046] (1) Fe 3 o 4 Preparation of nanospheres: fully dissolve 3g of ferric chloride hexahydrate in 70ml of ethylene glycol, slowly add 4.8g of anhydrous sodium acetate and 0.83g of sodium citrate, fully stir for 30min, then pour into the reaction kettle, and heat up to Keep at 200°C for 10h, then naturally lower to room temperature (such as 15°C), wash with water and alcohol three times, put it in an oven, and dry at 50°C for 6h to obtain Fe 3 o 4 nanospheres;
[0047] (2) Fe 3 o 4 @SiO 2 @PDA-Ni 2+ Preparation: Weigh the Fe prepared according to step (1) 3 o 4 100 mg of nanospheres, dispersed in a mixed solvent composed of 90 ml of ethanol and 15 ml of water, after ultrasonic dispersion for 30 min, add 2 mL of ammonia water with a mass fraction of 1%, place it in a magnetic field, stir for 5 min, and then add 200 μL of ethyl orthosilicate dropwise , after stirring in a magnetic field at room temperature for 17h, a mixture A was prepared; 15mg dopamine and 37.6mg NiC...
Embodiment 2
[0054] In order to prove the influence of the amount of TEOS (i.e. tetraethyl orthosilicate) on the degree of magnetically induced self-assembly ordering, under the same experimental conditions and steps as in Example 1, only the amount of TEOS was changed, and the amounts of TEOS were respectively Set to 100μL, 200μL, 400μL to obtain Fe with different thickness of silica 3 o 4 @SiO 2 and Fe 3 o 4 @SiO 2 @PDA-Ni 2+ , and finally the magnetic one-dimensional chain nanocomposite Fe 3 o 4 @SiO 2 @C / Ni.
[0055] figure 2 For the Fe prepared in Example 2 3 o 4 @SiO 2 The SEM and TEM images of , in which the images a and b respectively show the Fe 3 o 4 @SiO 2 The SEM and TEM images of Fig. 1, Fig. c and d respectively show the Fe 3 o 4 @SiO 2 The SEM and TEM images of the graphs, graphs e and f are respectively when the amount of TEOS is 400 μL, Fe 3 o 4 @SiO 2 SEM and TEM images. As can be clearly seen from the figure, the method described in Example 2 is ad...
Embodiment 3
[0057] In order to prove the influence of the magnetic field strength on the length of the one-dimensional chain of magnetically induced self-assembly, on the basis of the same experimental conditions and steps as in Example 1, only the strength of the magnetic field was changed, which were 300mT, 200mT and 150mT respectively, to obtain the one-dimensional chain length Different Fe 3 o 4 @SiO 2 @PDA-Ni 2+ , and after step (3) treatment, the magnetic one-dimensional chain nanocomposite Fe 3 o 4 @SiO 2 @C-Ni.
[0058] image 3 Fe obtained under different magnetic field strengths in the embodiment of the present invention 3 o 4 @SiO 2 The SEM and TEM images of @C / Ni, in which, images a and b are respectively Fe under a magnetic field strength of 300mT 3 o 4 @SiO 2 The SEM and TEM images of @C / Ni, Figures c and d are respectively Fe under the magnetic field strength of 200mT 3 o 4 @SiO 2 SEM and TEM images of @C / Ni, images e and f are respectively Fe under a magneti...
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