Method for preparing chemical raw material and liquid fuel from biomass
A technology for chemical raw materials and liquid fuels, used in the preparation of liquid hydrocarbon mixtures, petroleum industry, hydrotreating processes, etc., can solve the problems of difficult separation, easy oxidative deterioration and polycondensation, poor stability of bio-pyrolysis tar, etc. The effect of good catalytic activity, high conversion rate and innovative activation process
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Embodiment 1
[0030] Step 1. Use straw as biomass raw material. After pre-drying and crushing the straw, enter the rotary cone pyrolysis reactor for pyrolysis reaction. The operating temperature of biomass pyrolysis is 500°C, and the heating rate is 500°C / min. Pyrolysis products including pyrolysis gas, bio-tar, pyrolysis water and pyrolysis semi-coke were obtained; the distribution of the obtained pyrolysis products is shown in Table 1. Among them, the elemental analysis of biotar is shown in Table 2.
[0031] Step 2. The pyrolysis semi-coke obtained in step 1 is used as a carrier to prepare the first catalyst, the pyrolysis semi-coke is pre-ground to 40-200 mesh, and iron oxyhydroxide is used as an active component to prepare a slurry bed hydrogenation catalyst. Wherein, the ratio of active components and pyrolysis semi-coke is 0.5:1, and it is ready for use;
[0032] Step 3, the biotar obtained in step 1, the first catalyst obtained in step 2, and the hydrocarbon oil are made into a slu...
Embodiment 2
[0036] Step 1. Use the waste wood residue as biomass raw material. After pre-drying and crushing the waste wood residue, enter the rotary kiln pyrolysis reactor for pyrolysis reaction. The operating temperature of biomass pyrolysis is 300°C, and the heating rate is 100 °C / min to obtain pyrolysis products including pyrolysis gas, bio-tar, pyrolysis water and pyrolysis semi-coke. The distribution of the pyrolysis products obtained is shown in Table 1. Among them, the elemental analysis of biotar is shown in Table 2.
[0037] Step 2. The pyrolysis semi-coke obtained in step 1 is used as a carrier to prepare the first catalyst, the pyrolysis semi-coke is pre-ground to 40-200 mesh, and iron oxyhydroxide is used as an active component to prepare a slurry bed hydrogenation catalyst. Wherein, the ratio of active components and pyrolysis semi-coke is 0.6:1, and it is ready for use;
[0038] Step 3, the biotar obtained in step 1, the first catalyst obtained in step 2, and the hydrocar...
Embodiment 3
[0042] Step 1. Use municipal waste as biomass raw material. After sorting the municipal waste, take the recyclable waste for pre-drying and crushing, and then enter the fluidized bed pyrolysis reactor for pyrolysis reaction. The operating temperature of biomass pyrolysis is 600 °C, the heating rate is 600 °C / min, and pyrolysis products including pyrolysis gas, bio-tar, pyrolysis water and pyrolysis semi-coke are obtained. The distribution of the pyrolysis products obtained is shown in Table 1. Among them, the elemental analysis of biotar is shown in Table 2.
[0043] Step 2. The pyrolysis semi-coke obtained in step 1 is used as a carrier to prepare the first catalyst, the pyrolysis semi-coke is pre-ground to 40-200 mesh, and iron oxyhydroxide is used as an active component to prepare a slurry bed hydrogenation catalyst. Wherein, the ratio of active components and pyrolysis semi-coke is 0.6:1, and it is ready for use;
[0044] Step 3, the biotar obtained in step 1, the first ...
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