A lipoic acid-silver nano self-healing material and its preparation method and application
A self-healing material, lipoic acid technology, applied in the fields of botanical equipment and methods, applications, chemical instruments and methods, etc., can solve the problems of uneven distribution, complex synthesis or preparation process of self-healing materials, poor repeatability, etc.
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Embodiment 1
[0055] The preparation method of the lipoic acid-silver nanometer self-healing material of the present embodiment comprises the following steps:
[0056] (1) Dissolving lipoic acid in absolute ethanol according to the ratio of 1 g: 1 ml of lipoic acid and dehydrated ethanol to obtain lipoic acid solution;
[0057] (2) The lipoic acid solution is mixed with a concentration of 30mmol / L silver nitrate solution and reacted at 70°C for 10h to obtain a lipoic acid-silver nano self-healing material; wherein the volume ratio of the lipoic acid solution to the silver nitrate solution is 1 : 0.03.
Embodiment 2
[0059] The preparation method of the lipoic acid-silver nanometer self-healing material of the present embodiment comprises the following steps:
[0060] (1) Dissolving lipoic acid in absolute ethanol according to the ratio of 1 g: 1 ml of lipoic acid and dehydrated ethanol to obtain lipoic acid solution;
[0061] (2) The lipoic acid solution is mixed with a concentration of 30mmol / L silver nitrate solution and reacted at 70°C for 10h to obtain a lipoic acid-silver nano self-healing material; wherein the volume ratio of the lipoic acid solution to the silver nitrate solution is 1 : 0.15.
Embodiment 3
[0063] The preparation method of the lipoic acid-silver nanometer self-healing material of the present embodiment comprises the following steps:
[0064] (1) Dissolving lipoic acid in absolute ethanol according to the ratio of 1 g: 1 ml of lipoic acid and dehydrated ethanol to obtain lipoic acid solution;
[0065] (2) The lipoic acid solution is mixed with a concentration of 30mmol / L silver nitrate solution and reacted at 70°C for 10h to obtain a lipoic acid-silver nano self-healing material; wherein the volume ratio of the lipoic acid solution to the silver nitrate solution is 1 : 0.3.
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