Preparation method of composite conductive fabric
By adding functionalized carbon nanotubes and dendritic conductive particles to polyacrylonitrile fibers, the problems of easy shedding and insufficient strength of conductive fibers were solved, and a composite conductive fabric with high conductivity and high tensile strength was achieved, ensuring Long lasting conductive properties.
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Embodiment 1
[0032] A composite conductive fabric mainly includes the following raw material components in parts by weight: 40 parts of polyacrylonitrile, 6 parts of functionalized carbon nanotubes and 12 parts of conductive particles.
[0033] A kind of manufacture method of composite conductive fabric, the manufacture method of described composite conductive fabric mainly comprises following preparation steps:
[0034] (1) Mix sulfuric acid with a mass fraction of 95% and nitric acid with a mass fraction of 70% at a volume ratio of 3:1 to obtain a mixed acid solution, mix the mixed acid solution with carbon nanotubes at a mass ratio of 10:1, and heat at temperature After stirring and reacting for 3 hours under the conditions of 45° C. and a rotating speed of 300 r / min, filter to obtain a functionalized carbon nanotube blank, wash the functionalized carbon nanotube blank 8 times with deionized water, and place it in a room at a temperature of 85° C. Dry for 3 hours under the condition;
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Embodiment 2
[0042] A composite conductive fabric mainly includes the following raw material components in parts by weight: 40 parts of polyacrylonitrile and 12 parts of conductive particles.
[0043] A kind of manufacture method of composite conductive fabric, the manufacture method of described composite conductive fabric mainly comprises following preparation steps:
[0044] (1) Mix porous silica and mixed acid solution at a mass ratio of 1:8, stir and react for 1 hour at a temperature of 45°C and a rotation speed of 300r / min, and then filter to obtain pretreated porous silica. Mix the pretreated porous silica and the mixed lye at a mass ratio of 1:8, stir and react for 1 hour at a temperature of 45°C and a rotation speed of 300r / min, and then filter to obtain a modified silica blank. After the silica blank was washed 5 times with deionized water, and dried for 2 hours at a temperature of 70°C, the modified silica was obtained, and the modified silica was mixed with 10% polyallylamine s...
Embodiment 3
[0051] A composite conductive fabric mainly includes the following raw material components in parts by weight: 40 parts of polyacrylonitrile, 6 parts of functionalized carbon nanotubes and 12 parts of conductive particles.
[0052] A kind of manufacture method of composite conductive fabric, the manufacture method of described composite conductive fabric mainly comprises following preparation steps:
[0053] (1) Mix sulfuric acid with a mass fraction of 95% and nitric acid with a mass fraction of 70% at a volume ratio of 3:1 to obtain a mixed acid solution, mix the mixed acid solution with carbon nanotubes at a mass ratio of 10:1, and heat at temperature After stirring and reacting for 3 hours under the conditions of 45° C. and a rotating speed of 300 r / min, filter to obtain a functionalized carbon nanotube blank, wash the functionalized carbon nanotube blank 8 times with deionized water, and place it in a room at a temperature of 85° C. Dry for 3 hours under the condition;
...
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Abstract
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