Nano plugging agent for water plugging of oil well and preparation method thereof
A nano-blocking agent and oil well water plugging technology, which is applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve problems such as difficult water plugging, difficult section blocking, thin oil layers, etc., to increase salt resistance, Good thermal stability and little influence of rheology
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Embodiment 1
[0031] The present invention provides such as figure 1 Shown is a nano-blocking agent for oil well water plugging, the plugging agent is prepared from the following raw materials:
[0032] The raw materials are: 15 parts of sol, 6 parts of polyacrylamide, 1.6 parts of nano silicon dioxide, 0.42 parts of emulsifier, 3 parts of sodium chloride, 0.35 parts of NS-6 and 0.6 parts of tackifier.
[0033] Specifically in the present invention: the emulsifier is fatty acid soap, and by adding the emulsifier, the API and high-temperature and high-pressure fluid loss of the drilling fluid can be significantly reduced.
[0034] Specifically in the present invention: the sol is prepared from the following raw materials in parts by weight: 7 parts of metal alkoxide, 4 parts of water, 2 parts of solvent, and 0.8 part of catalyst. Metal alkoxide is the most suitable raw material for the sol-gel method, providing metal elements , to improve the strength of the sol, water is the necessary raw ...
Embodiment 2
[0052] A nano plugging agent for oil well water plugging, the plugging agent is prepared from the following raw materials:
[0053] The ratio of raw materials by weight is: 20 parts of sol, 7 parts of polyacrylamide, 2.6 parts of nano silicon dioxide, 0.56 parts of emulsifier, 3.5 parts of sodium chloride, 0.45 parts of NS-6 and 1.3 parts of tackifier.
[0054] Specifically in the present invention: the emulsifier is any one or more mixtures of fatty acid soaps, alkyl sulfates, alkylbenzenesulfonates and phosphates.
[0055] Specifically in the present invention: the sol is prepared from the following raw materials in parts by weight: 8 parts of metal alkoxide, 6 parts of water, 4 parts of solvent, and 0.9 part of catalyst.
[0056] Specifically in the present invention: the solvent is butanol, and the catalyst is succinic acid and maleic acid.
[0057] A preparation method of nano plugging agent for oil well water plugging, comprising the following steps:
[0058] Step 1. A...
Embodiment 3
[0069] A nano plugging agent for oil well water plugging, the plugging agent is prepared from the following raw materials:
[0070] Raw materials in parts by weight are: sol 25 parts, polyacrylamide 8 parts, nano silicon dioxide 3.6 parts, emulsifier 0.68 parts, sodium chloride 4 parts, NS-6: 0.55 parts and tackifier 3.4 parts.
[0071] Specifically in the present invention: the emulsifier is any one or more mixtures of fatty acid soaps, alkyl sulfates, alkylbenzenesulfonates and phosphates.
[0072] Specifically in the present invention: the sol is prepared from the following raw materials in parts by weight: 9 parts of metal alkoxide, 8 parts of water, 6 parts of solvent, and 1.5 parts of catalyst.
[0073] The present invention is specific: the solvent is ethylene oxide, and the catalyst is hydrochloric acid.
[0074] A preparation method of nano plugging agent for oil well water plugging, comprising the following steps:
[0075] Step 1. Add the sol and polyacrylamide int...
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