Glyphosate compound aqueous solution as well as preparation method and application thereof

A glyphosate and water preparation technology, which is applied in the field of glyphosate compound water preparation and its preparation, can solve the problems of pesticide residues, plant phytotoxicity, environmental pollution, difficulty in degradation, and increase in the amount of chemical pesticide components, and achieves a good market. Prospect, low cost, effect of increased suppression rate

Active Publication Date: 2021-12-03
HANGZHOU JINFADA CHEM IND +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

my country has 16 compounding certificates for the registration of glyphosate compounding. Glyphosate compounding has achieved certain results, but all of the registered compound herbicides are chemical ...

Method used

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  • Glyphosate compound aqueous solution as well as preparation method and application thereof
  • Glyphosate compound aqueous solution as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] (1), prepare walnut leaf aqueous extract

[0032] Dry and pulverize walnut leaves, add water and soak at room temperature for 0.5h, the mass ratio of walnut leaves to water is 1g: 25ml, filter, extract the filtrate with anhydrous ether for 3 times, combine organic phases, and precipitate to obtain walnut leaves Flavonoid extract; standby;

[0033] (2), preparation of vinca alkaloids

[0034] S1, periwinkle is put into the oven of 80 ℃ and dried for 2h, pulverized, and extracted with ethanol with a mass percentage concentration of 70% at normal temperature. The solid-liquid ratio of periwinkle and ethanol is 1g:10ml, and the extraction time is 20h. filter paper, and collect the filtrate and filter residue respectively;

[0035]S2, the filter residue in step S1 is leached again with the ethanol of mass percentage concentration 20% at 60 DEG C of temperature assisted leaching 20min, the power of ultrasonic wave is 300W, the solid-liquid ratio of filter residue and ethano...

Embodiment 2

[0041] (1), prepare walnut leaf aqueous extract

[0042] Dry and pulverize walnut leaves, add water and soak at room temperature for 0.8h, the mass ratio of walnut leaves to water is 1g:25ml, filter, extract the filtrate with ethyl acetate for 3 times, combine organic phases, and precipitate to obtain walnut leaves Flavonoid extract; standby;

[0043] (2), preparation of vinca alkaloids

[0044] S1, periwinkle is put into the oven of 83 ℃ and dried for 2.2h, pulverized, and extracted with ethanol with a mass percentage concentration of 75% at room temperature. Filter with filter paper, collect filtrate and filter residue respectively;

[0045] S2, the filter residue in the step S1 is leached again with the ethanol of mass percentage concentration 22% at 65 DEG C temperature for 20min, the ultrasonic power is 350W, the solid-liquid ratio of filter residue and ethanol is 1g:5.5ml, filter, collect Filtrate, combining the filtrate and the filtrate in step S1 to obtain two extra...

Embodiment 3

[0051] (1), prepare walnut leaf aqueous extract

[0052] Dry and pulverize walnut leaves, add water and soak at room temperature for 1.0h, the mass ratio of walnut leaves to water is 1g:28ml, filter, extract the filtrate with ethyl acetate for 3 times, combine the organic phases, and precipitate to obtain walnut leaves Flavonoid extract; standby;

[0053] (2), preparation of vinca alkaloids

[0054] S1, periwinkle flower is put into the oven of 85 ℃ and dried for 2.5h, pulverized, and extracted with ethanol with a mass percentage concentration of 80% at room temperature, the solid-liquid ratio of periwinkle flower and ethanol is 1g:13ml, and the extraction time is 22h, and is extracted with gauze Filter with filter paper, collect filtrate and filter residue respectively;

[0055] S2, the filter residue in step S1 is leached again with the ethanol of mass percentage concentration 25% at 70 ℃ of temperature assisted leaching 25min by ultrasonic wave, the power of ultrasonic wa...

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Abstract

The invention discloses a glyphosate compound aqueous agent. The glyphosate compound aqueous agent comprises the following main active components: glyphosate, a walnut leaf aqueous extract and catharanthus roseus alkaloid, and the compound aqueous agent is prepared from the following raw materials in parts by weight: 15 to 20g of glyphosate, 5 to 8g of walnut leaf water extract, 4 to 6g of catharanthus alkaloid, 1 to 2g of a solubilizer, 0.5 to 1g of a stabilizer and 500 to 600mL of water. Meanwhile, the invention further discloses a preparation method of the glyphosate compound aqueous solution and application of the glyphosate compound aqueous solution. The use amount of chemical pesticides is reduced, meanwhile, the defects that biological pesticides are slow in speed and high in use cost are overcome, crops are effectively protected from being invaded by pests, much pollution and damage to the ecological environment are avoided, the weeding spectrum is expanded, the weeding effect is improved, the weeding speed of glyphosate is increased, and the weeding composition has a good market prospect.

Description

technical field [0001] The invention belongs to the technical field of pesticide preparations, and in particular relates to a glyphosate compound water preparation and its preparation method and application. Background technique [0002] Glyphosate, the chemical name is N-(phosphomethyl)glycine, and the chemical formula is C 3 h 8 NO 5 P, is an environmentally friendly systemic conduction type broad-spectrum herbicide, which has a very good effect on perennial weeds and biennial grass weeds. Due to its excellent herbicidal activity, broad herbicidal spectrum, low soil residue, long weed control time, and the mass planting of herbicide-resistant transgenic crops, glyphosate has become the world's No. 1 herbicide in sales Variety. However, in recent years, the long-term, single, continuous, and extensive use of glyphosate has led to an increase in resistant weed individuals and populations, reducing the control effect of herbicides and increasing the cost of weed control. ...

Claims

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Application Information

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IPC IPC(8): A01N65/08A01N57/20A01N43/90A01N25/02A01P13/00C07D519/04
CPCA01N65/00A01N65/08A01N57/20A01N43/90A01N25/02C07D519/04
Inventor 刘开孟韩晓丹李斌严郭新周锦枫祝建浩刘劭农钟桂芳
Owner HANGZHOU JINFADA CHEM IND
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