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Quality control method of Chinese medicinal preparation

A quality control method and preparation technology, applied in the direction of testing pharmaceutical preparations, pharmaceutical formulations, measuring devices, etc., can solve the problems of ineffective control of the quality of antithrombotic preparations, affecting product production and quality assurance

Inactive Publication Date: 2006-06-14
GUIZHOU YIBAI PHARMA CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, existing quality control methods cannot effectively control the quality of antithrombotic preparations, which will affect the production and quality assurance of products.

Method used

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  • Quality control method of Chinese medicinal preparation
  • Quality control method of Chinese medicinal preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0132] Embodiment 1 antithrombotic capsule

[0133] [Prescription] 200g angelica tail, 200g salvia miltiorrhiza, 100g silkworm (stir-fried bran), 100g gecko, 200g ground beetle, 50g centipede, 200g leech, 100g hive, 100g earthworm, 30g nux (made) , 3g musk, toad venom (made of wine) 1g, 100g of licorice, 200g of Smilax cocos, 100g of corydalis (made of vinegar), 200g of drynaria (made of wine), 200g of black snake (made of wine), 50g of horsefly (de-winged), 50g of pangolin (sand hot) 50g

[0134] [Preparation method] The above raw materials, except musk and toad venom, other seventeen flavors such as angelica tail, are crushed into fine powder, the musk and toad venom are ground into fine powder, mixed with the above powder, sieved, mixed evenly, and put into capsules. have to.

[0135] 【identification】

[0136] (1) Take 2g of the content of the antithrombotic capsule and observe it under a microscope: the mycelium is nearly colorless, slender and curled and entangled in ...

Embodiment 2

[0155] Embodiment 2 antithrombotic tablet

[0156] [Prescription] 200g angelica tail, 200g salvia miltiorrhiza, 100g silkworm (stir-fried bran), 100g gecko, 200g ground beetle, 50g centipede, 200g leech, 100g hive, 100g earthworm, 30g nux (made) , 3g musk, toad venom (made of wine) 1g, 100g of licorice, 200g of Smilax cocos, 100g of corydalis (made of vinegar), 200g of drynaria (made of wine), 200g of black snake (made of wine), 50g of horsefly (de-winged), 50g of pangolin (sand hot) 50g

[0157] [Preparation method] The above raw materials, except musk and toad venom, other seventeen flavors such as angelica tail, are crushed into fine powder, and the musk and toad venom are ground separately, mixed with the above powder, sieved, mixed, granulated, and conventionally Made into tablets, 0.4g / tablet, ready to use.

[0158] [Quality Control Method] Identification and content determination methods are the same as in Example 1, wherein each piece of content contains Danshen and ...

Embodiment 3

[0159] Example 3 Antithrombotic Granules

[0160] [Prescription] 200g angelica tail, 200g salvia miltiorrhiza, 100g silkworm (stir-fried bran), 100g gecko, 200g ground beetle, 50g centipede, 200g leech, 100g hive, 100g earthworm, 30g nux (made) , 3g musk, toad venom (made of wine) 1g, 100g of licorice, 200g of Smilax cocos, 100g of corydalis (made of vinegar), 200g of drynaria (made of wine), 200g of black snake (made of wine), 50g of horsefly (de-winged), 50g of pangolin (sand hot) 50g

[0161] [Preparation method] The above raw materials, except musk and toad venom, the other seventeen flavors such as angelica tail, are ground into fine powder, the musk and toad venom are ground into fine powder, mixed with the above powder, sieved, mixed, and made into granules by conventional methods Dosage, 5g / bag. Instantly.

[0162] [Quality Control Method] Identification and content determination methods are the same as in Example 1, wherein each bag of content contains Salvia milti...

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Abstract

A quality control method for the Chinese medicine to treat thrombus features that a thin-layer chromatography is used for the identification to earthworm, vomiting nut, musk, corydalis tuber, toad, liquorice root, etc and an efficient liquid-phase chromatography is used to measure the contents of tanshinone IIA and strychnine.

Description

Technical field: [0001] The invention relates to a quality control method for traditional Chinese medicine preparations, in particular to a quality control method for antithrombotic preparations. Background technique: [0002] The raw materials of antithrombotic preparations are composed of angelica tail, salvia miltiorrhiza, silkworm, gecko, wood beetle, centipede, leech, honeycomb, earthworm, nuxya, musk, toad, licorice, soil tuckahoe, corydalis, rhizoma drynaria, black shoot Composed of nineteen traditional Chinese medicines such as snake, horsefly, pangolin, etc., there are many dosage forms in the market in China. However, we found through our research that the existing antithrombotic preparations have the disadvantages of backward quality control methods and difficult control of product quality. In the existing quality control methods, there is no identification of Angelica tail, Earthworm, Strychnium, Musk, Corydalis, Toad and Licorice, or content determination of ta...

Claims

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Application Information

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IPC IPC(8): A61K36/90A61K35/55A61K35/583A61K35/64A61K35/648A61K35/65A61P7/02G01N30/02G01N33/15
Inventor 叶湘武王泽坤
Owner GUIZHOU YIBAI PHARMA CO LTD
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