The invention belongs to the technical field of cotton fabric after-finishing of the
dyeing and finishing industry, and particularly relates to a preparation method of low-
formaldehyde easy-care resin. The method comprises the steps that firstly, a
formaldehyde solution reacts with first-batch
urea, then, first-stage quantified
distillation is performed, after
distillation is completed, second-batch
urea is added for a reaction, and then, second-stage quantified
distillation is performed to obtain a dimethylol
ethylene urea solution; deionized water and
glyoxal are added into the solution fora reaction till the residual quantity of
glyoxal in the solution is smaller than 0.8%, and cooling is performed; finally,
alcohol substances are added, cooling is performed, ammoniac derivatives are added, the pH value is regulated to 5.0-7.0, and low-
formaldehyde easy-care resin is obtained. According to the preparation method of the low-formaldehyde easy-care resin, the preparation method is simple, the cost is low, industrial production can be achieved, compared with common 2D resin, the prepared low-formaldehyde easy-care resin has the low
strength loss and the high value of whiteness, andthe easy-care performance equivalent to the common 2D resin can be achieved.