Biphenthrin dichlorvos compound insecticide
A technology of bifenthrin and dichlorvos, applied in the directions of pesticides, biocides, animal repellents, etc., to achieve the effects of reducing pollution, reducing drug costs, and reducing pesticide residues
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Embodiment 1
[0021] The preparation of 40% bifenthrin dichlorvos emulsifiable concentrate (the ratio of the original drug of bifenthrin and the original drug of dichlorvos in the active pharmaceutical ingredients is 1:1):
[0022] Auxiliary selection: DMF, Nongru 0206, Nongru 2201.
[0023] Solvent of choice: Toluene.
[0024] Each component is prepared according to the following percentages by weight:
[0025] Bifenthrin: 20%; Dichlorvos: 20%; DMF 5%; Nongru 1205: 5%; Nongru 0206: 5%; solvent: toluene, add to 100g.
[0026] Preparation process: Dissolve bifenthrin with a small amount of acetone, then add dichlorvos, DMF, Nongru 1205, and Nongru 0206 in sequence, then fill it with toluene to 100%, mix the above mixture in a volumetric flask to obtain 40% biphenyl Permethrin dichlorvos EC.
Embodiment 2
[0028] The preparation of 40% bifenthrin dichlorvos aqueous suspension (the ratio of the original drug of bifenthrin and the original drug of dichlorvos in the active pharmaceutical ingredient is 1: 3):
[0029] Auxiliary selection: sodium lignosulfonate, OP-10; CMC; organosilicone; ethylene glycol.
[0030] Solvent of choice: water.
[0031] Each component is prepared according to the following weight percentages:
[0032] Bifenthrin: 10%; Dichlorvos: 30%; Sodium lignosulfonate: 10.0%; OP-10: 5.0%; Thickener CMC: 1.0%; Defoamer organic silicone: 0.01%; Antifreeze B Diol: 8.0%; Water: add to 100 g.
[0033] Preparation process: put bifenthrin, dichlorvos, sodium lignosulfonate, OP-10, thickener CMC, defoamer organic silicone, antifreeze ethylene glycol in the reaction kettle according to the above ratio, add water to Mix 100% evenly, then introduce the mixture into a sand mill and grind until the material fineness is 1-5 μm; after grinding, mix evenly to form a water suspen...
Embodiment 3
[0035] Tested pesticide: 40% bifenthrin dichlorvos emulsifiable concentrate (provided in Example 1);
[0036] Control pesticide: 10% bifenthrin emulsifiable concentrate (self-made), 40% dichlorvos emulsifiable concentrate (self-made);
[0037] Insects for testing: 2 instar diamondback moth larvae (indoor rearing of Jiangsu Academy of Agricultural Sciences);
[0038] Determination method: insect dipping method.
[0039] Insect soaking method: the test drug solution was diluted into 5 concentration gradients, 20 2-instar diamondback moth larvae were immersed in the drug solution for 15 seconds, taken out and dried, and then inserted into a petri dish with fresh and non-polluting vegetable leaves. Treat 3 repetitions. At the same time, water was used as a control treatment. After 24 hours, check the number of living insects, calculate the corrected mortality rate, and calculate the lethal concentration (LC 50 ).
[0040] Toxicity determination method of 40% bifenthrin dichlo...
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