Method for preparing nontoxic coloured silicasol
A silica sol and colored technology, which is applied in the field of preparation of non-toxic colored silica sol, can solve the problems of inability to colorize, and the application of coloring cannot meet the requirements, and achieves the effects of strong colorability, stable properties and convenient operation.
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[0028] Preferred embodiment of the present invention: Add 0.25 kg of elemental silicon powder with a particle size of 200 mesh and 20 grams of catalyst in 3.5 kg of deionized water, heat to 90 ° C, stir at a constant speed of 100 rpm, and drop the concentration of 28% every two hours 5ml of ammonia water, stop dripping ammonia water after four hours, and colorless silica sol is obtained. Adjust the pH of the colorless silica sol to 2-4 with a 5% hydrochloric acid solution, and then add FeCl with a molar concentration of 0.3mol / l 3 0.2 kg of aqueous solution, continue to heat and stir for 8 hours, filter, stir and concentrate at 150°C until the solution concentration is 15-20%, that is, a non-toxic colored silica sol is obtained.
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