Novel use of fraxinellone and fraxinellone aqua pesticide

An insecticide and a technology for preparing insecticides, applied in the direction of nematicides, applications, biocides, etc., can solve problems such as unseen research, and achieve an effect that is conducive to environmental protection and ecological balance

Inactive Publication Date: 2008-07-30
原春兰
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Alkaloids are generally considered to be active chemical components, but the biological activities of Limonoids (limonoids) and Degraded limonoids (degradable limonoids) contained in Rutaceae and Meliaceae plants have aroused people's attention. Widely concerned, Fraxinellone isolated from neem bark is a Degradedlimonoids, its biological activity has been reported, but there is no research on the preparation of Fraxinellone obtained from white moss bark into botanical pesticides

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment Construction

[0017] 1, the extraction method of arketone in the white moss bark.

[0018] Weigh 10 kg of white moss bark powder, moisten with 10 times the amount of lye without sticking hands, add an appropriate amount of petroleum ether to soak for 24 hours, add 10 times the amount of petroleum ether to reflux extraction three times, each time for 1.5 hours, and suction filter. The filtrates were combined and concentrated to dryness to obtain a petroleum ether extract. Add the above extract to a mixed solvent of methanol:petroleum ether=3:1, separate with a separatory funnel, discard the fat-soluble components in the upper layer, and the white needle-like crystals will crystallize from the methanol in the lower layer solution, and recrystallize through methanol to obtain ash Crude ketones.

[0019] The crude product was further purified by column chromatography using cyclohexane: ethyl acetate = 3:2 as the eluent and recrystallized from methanol to obtain the fine alkone. The content of...

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PUM

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Abstract

The invention relates to a novel usage of fraxinellon and an insecticide of water aqua of fraxinellon, in particular to the application of fraxinellon in preparing the insecticide. The insecticide in the invention is a solvent extract of a root bark of Dictamnus dasycarpus Turcz. The insecticide of water aqua of fraxinellon in the invention is an insecticide of water aqua made with fraxinellon as an active component, which is prepared by the raw materials with a weight percentage as: 7 to 8 percent of fraxinellon, 10 to 13 percent of emulsifier, 15 to 20 percent of solvent the rest is water. The invention is of high effect, low toxicity, pollution-free and is easy to degrade and compatible with the environment. Through the experiment in large fields, the 75G/L insecticide of water aqua of fraxinellon has a certain prevention effect on the diamondback moth, while the prevention effects of the liquids with 200 times, 300 times and 500 times of the 75G/L insecticide of water aqua of fraxinellon are respectively 65.46 percent, 61.45 percent and 54.55 percent. The drug effects are increased by a certain extent after being controlled for seven days which respectively reach 70.42 percent, 64.50 percent and 59.70 percent.

Description

technical field [0001] The invention relates to a new application of arketone and an arketone aqueous insecticide. Background technique [0002] The inherent disadvantages of chemical pesticides and people's irrational long-term abuse, their toxic side effects and negative impact on the environment and ecological balance are beyond doubt. With people's understanding of pesticides and the emergence of toxic and side effects of chemical pesticides on humans, animals and the environment, natural plant-derived pesticides are favored by people. [0003] Among the nearly 30,000 species of higher plants in my country, nearly a thousand plants have insecticidal activity. The active ingredients of these plants not only have good insecticidal effect, are safe and easy to degrade crops, have a short residual effect period, and are not easy to produce drug resistance. As a plant source Pesticides have broad prospects. However, only 10% of people have studied their chemical properties, a...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A01N43/08A01N25/04A01P7/00A01P5/00
Inventor 原春兰王晓玲杨德锁
Owner 原春兰
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