Method for measuring heavy metal in sea water by ion color spectrum flow injection chemiluminescence restraint method
A flow injection and chemiluminescence technology, applied in the field of environmental chemical monitoring, can solve the problems of long analysis duration, inability to work on site, complicated analysis process, etc., and achieve the effect of high sensitivity and fast analysis speed.
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[0034] The inventive method comprises the following steps:
[0035] (1). Utilize the electrolytic type ozone generator 2 to produce the ozone solution of stable concentration, make the ozone solution flow through the ozone solution balance chamber 7 by the pump 8, the ozone solution dynamic balance tube 6 made of optical glass is housed in the ozone solution balance chamber 7, in An ultraviolet lamp 5 is arranged on its side. When the ozone solution flows through the dynamic balance tube 6, the ozone solution is irradiated by the ultraviolet lamp 5 and partially decomposed to generate hydroxyl radicals. The hydroxyl radicals and ozone can be used as an oxidant to oxidize the luminescent reagent 9 together.
[0036] (2). After the ozone solution flows through the dynamic balance tube 6 of the ozone solution, it is mixed with the luminescent reagent-rhodamine B9 as the carrier.
[0037] (3). The sample peristaltic pump 14 transports the sample 13 to the quantitative tube of the ...
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