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Method for producing high-efficient defluorination active micropore ceramic stuffing

A microporous ceramic and active technology, applied in inorganic chemistry, adsorption water/sewage treatment, non-metallic elements, etc., can solve the problems of discounted defluoridation effect and increased water flow resistance, and achieve strong defluoridation ability and long service life , the effect of low operating cost

Inactive Publication Date: 2010-11-03
宜兴市得力陶瓷科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The disadvantage is that in order to increase the specific surface area and avoid the increase of water flow resistance caused by the excessive density of the supporting filter, the particle size of each material must be strictly controlled during the proportioning, especially the uniform mixing. In the actual use process, under the impact of water flow, It is unrealistic to keep the adsorbent in a uniformly mixed state all the time. The deviation of the components of the adsorbent during use causes some water flow to only pass through some of the components, which greatly reduces the defluoridation effect.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0009] Example 1, a preparation method of high-efficiency defluoridation active microporous ceramic filler, 30 parts of 200-mesh medical stone, 55 parts of 200-mesh zeolite, 15 parts of 180-mesh pottery clay and water are uniformly mixed, and extruded into 1-3mm particles , after drying, roast at 1250°C-1300°C for 3-4 hours, after cooling, put it in a caustic soda solution with a mass concentration of 5-10% and boil for 8-10 hours, take it out and wash it to neutral, and then put it in Soak in dilute sulfuric acid with a mass concentration of 1-5% for 4-5 hours, take it out, clean it and dry it.

Embodiment 2

[0010] Embodiment 2, with reference to Example 1, the parts of medical stone, zeolite and pottery clay are respectively 32 parts, 51 parts and 17 parts.

Embodiment 3

[0011] Embodiment 3, referring to Example 1, the parts of medical stone, zeolite and pottery clay are respectively 30 parts, 50 parts and 20 parts.

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PUM

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Abstract

The invention discloses a method for preparing a microporous ceramic packing capable of removing fluorine activity with high efficiency, and relates to a method for preparing a water treatment material. The method comprises the following steps: 200 meshes of medical stone, 200 meshes of zeolite, 180 meshes of clay, and water are evenly mixed; the weight percentage of the raw materials is as follows: 30 to 35 percent of the medical stone, 50 to 55 percent of the zeolite, and 15 to 20 percent of the clay; the raw materials are extruded into particles with the size of between 1 and 3mm; the particles are roasted at a temperature of between 1,250 and 1,300 DEG C for 3 to 4 hours after being dried, and are boiled in caustic soda solution for 8 to 10 hours after being cooled down; the particlesare soaked in dilute sulfuric acid for 4 to 5 hours after being taken out, cleaned and neutralized; and then the particles are taken out, cleaned and dried. The packing has the advantages that the packing has low operating cost and a long service cycle and can be regenerated and reused through the treatments such as roasting, soda boiling, acid dipping, and the like after being used for a long time.

Description

technical field [0001] The invention belongs to a preparation method of a water treatment material, in particular to a preparation method of an active microporous ceramic filler capable of efficiently removing fluorine. Background technique [0002] Fluorine is a widely distributed element in the formation, which has a strong affinity and ore-forming ability. Differences in fluorine-containing mineral components and natural conditions in different regions lead to uneven regional distribution of fluorine. In areas with high fluorine content in water, fluorine greatly endangers the health of local people and is one of the serious endemic diseases in our country. If a kind of adsorption material with good fluoride removal effect and economical and practical can be produced, it will be a reasonable way to promote the use of fluoride removal in drinking water, and it will definitely play a positive role in the prevention and treatment of endemic fluorosis, especially for local d...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J20/10C02F1/28
Inventor 王德君周新
Owner 宜兴市得力陶瓷科技有限公司