Photosemiconductor package sealing resin material
一种光半导体、密封树脂的技术,应用在半导体器件、半导体/固态器件零部件、电固体器件等方向,能够解决机械性能劣化等问题,达到良好透明性、高触变性、良好耐裂性的效果
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[0044] Next, the present invention will be described more specifically by way of examples.
reference example 1
[0046] (Preparation of Epoxy-Clay Mineral Dispersion Using Hydrophobic Hectorite)
[0047] 5 g of hectorite (Lucentito SEN, Cop Chemical Co., Ltd.), which is a synthetic smectite, was added to 100 g of toluene, stirred at room temperature for 6 hours and dispersed to obtain a viscous clay mineral dispersion. It should be noted that the chemical formula of hectorite uses Na 0.33 (Mg 2.67 Li 0.33 ) Si 4 o 10 (OH) 2 Indicates that the hydrophobic hectorite used is a hectorite in which polyoxyethylene or alkylmethylammonium ions are intercalated.
[0048] The obtained clay mineral dispersion was added to the epoxy dispersion obtained by dispersing 45 g of liquid hydrogenated bisphenol A type epoxy compound (YX8000, Japan Epikisilesin Co., Ltd.) in 100 g of dimethylformamide in advance. After stirring for 24 hours, a colorless and transparent epoxy dispersion was obtained.
[0049] By concentrating the resulting epoxy dispersion under reduced pressure with an evaporator, an ...
reference example 2
[0051] (Preparation of Epoxy-Clay Mineral Dispersion Using Hydrophobic Bentonite)
[0052] 5 g of bentonite (Esben NX, Hogyun Co., Ltd.), which is a synthetic smectite, was added to 100 g of toluene, and stirred at room temperature for 6 hours to disperse to obtain a viscous clay mineral dispersion. It should be noted that the chemical formula of bentonite varies according to the synthesis conditions, but generally Na 0~0.66 Ca 0~0.66 (Mg 0~0.66 Al 3.34 ) Si 8 o 20 (OH) 4 It shows that the hydrophobic bentonite used is bentonite with trioctylammonium ions intercalated between layers.
[0053] The obtained clay mineral dispersion was added to an epoxy dispersion previously obtained by dispersing 45 g of a liquid hydrogenated bisphenol A epoxy compound (YX8000, Japan Epikisilesin Co., Ltd.) into 100 g of toluene, and stirred at room temperature for 24 hours. A colorless and transparent epoxy dispersion was obtained.
[0054] By concentrating the resulting epoxy dispersio...
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