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Application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole in preparation of insecticide
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A technology for the preparation and application of insecticides, applied in the direction of insecticides, applications, and biocides, which can solve the problems of no research reports on applications
Inactive Publication Date: 2013-05-08
CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY
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There is no research report on the application of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole in the preparation of insecticides
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Embodiment 1
[0011] Example 1 Preparation of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole (I)
[0012] Prepare 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole (I ):
[0015] Example 2 Determination of the insecticidal activity of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole
[0016] 1. Purpose of the test: To determine the toxicity of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole to Vicia faba aphid at the test concentration in the room Evaluation of its insecticidal activity.
[0017] 2 test conditions
[0018] 2.1 Test target: broad bean aphid (Aphis fabae) is a sensitive strain that has been raised indoors with broad bean seedlings for many years, and the test insects are 3-day-old nymphs.
[0019] 2.2 Culture conditions: The culture conditions of the test target and the test target are temperature 25±5°C, relative humidity 65±5%, and light cycle 12 / 12h (L / D).
[0020] 2.3 Instruments and equipment: electronic balance (sensitivity 1 / 10,000), 100ml beaker, measuring cylinder, petri dish, paramembrane, sponge, filter paper, pipette, tweezers, brush, etc.
[0021] 3 Experimental design
[0022] 3.1 Preferred compoun...
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Abstract
The invention discloses application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole as shown in a chemical structural formula I in the preparation of insecticides, wherein X in the chemical structural formula I is selected from hydrogen, 2-chlorine, 2-fluorine, 2-hydroxy, 2-methoxyl, 2-ethyoxyl, 2-nitryl, 3-dimethylamino, 3-chlorine, 3-bromine, 3-fluorine, 3-methyl, 3-ethyl, 3-trifluoromethyl, 3-hydroxy, 3-methoxyl, 3-ethyoxyl, 3-nitryl, 3-sulfonic group, 3-methanesulfonylamino, 3-sulfamoyl, 4-dimethylamino, 4-chlorine, 4-bromine, 4-fluorine, 4-methyl, 4-ethyl, 4-trifluoromethyl, 4-hydroxy, 4-methoxyl, 4-ethyoxyl, 4-acetoxyl group, 4-nitryl, 4-sulfonic group, 4-methanesulfonylamino, 4-sulfamoyl, 2-chlorine-5-nitryl, 3-ethyl-4-hydroxy, 3,4-dimethoxy, 2,4-dichloro, 2-hydroxy-5-bromine, 2-hydroxy-5-iodine, 2-hydroxy-5-chlorine, 2,4-difluoro, 2-hydroxy-3,5 dibromo, 2-hydroxy-3,5 diiodo, 2-hydroxy-3,5 dichloro or 2-hydroxy-3,5 difluoro.
Description
technical field [0001] The present invention relates to the application of a class of compounds in the preparation of insecticides, specifically 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole in the preparation of insecticides application in agents. Background technique [0002] Azole heterocyclic derivatives have always been paid attention to by drug and pesticide workers because of their good biological activity, high drug efficacy, wide bactericidal spectrum, and good systemic property [Comperhensive Heterocylie Chemistry. Pergamon Oxford, 1983, 5: 733-735], and triazoles are one of the more influential ones. The bactericidal mechanism of triazole fungicides is to affect the formation of fungal cell walls by hindering the biosynthesis of fungal ergosterol, and have good control effects on most fungal diseases that endanger crop growth. Triazole fungicides also have certain plant growth regulating activity [Pesticides, 1994, 33 (4): 19-20; J Med Chem, 1996, 39 (...
Claims
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Patent Type & Authority Patents(China)
IPC IPC(8): A01N43/78A01P7/04A01P13/00
Inventor 陈平龙姝霍素芳沈芳
Owner CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY
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