Application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole in preparation of insecticide

A technology for the preparation and application of insecticides, applied in the direction of insecticides, applications, and biocides, which can solve the problems of no research reports on applications

Inactive Publication Date: 2013-05-08
CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY
View PDF3 Cites 2 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

There is no research report on the application of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole in the preparation of insecticides

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole in preparation of insecticide
  • Application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole in preparation of insecticide
  • Application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole in preparation of insecticide

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0011] Example 1 Preparation of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole (I)

[0012] Prepare 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole (I ):

[0013]

[0014] X is selected from: hydrogen, 2-chloro, 2-fluoro, 2-hydroxy, 2-methoxy, 2-ethoxy, 2-nitro, 3-dimethylamino, 3-chloro, 3-bromo, 3 -Fluoro, 3-methyl, 3-ethyl, 3-trifluoromethyl, 3-hydroxy, 3-methoxy, 3-ethoxy, 3-nitro, 3-sulfonic acid, 3-methyl Sulfonylamino, 3-sulfamoyl, 4-dimethylamino, 4-chloro, 4-bromo, 4-fluoro, 4-methyl, 4-ethyl, 4-trifluoromethyl, 4-hydroxyl, 4 -methoxy, 4-ethoxy, 4-acetoxy, 4-nitro, 4-sulfonate, 4-methanesulfonylamino, 4-sulfamoyl, 2-chloro-5-nitro, 3-Ethyl-4-hydroxy, 3,4-dimethoxy, 2,4-dichloro, 2-hydroxy-5-bromo, 2-hydroxy-5-iodo, 2-hydroxy-5-chloro, 2 , 4-difluoro, 2-hydroxy-3,5 dibromo, 2-hydroxy-3,5 diiodo, 2-hydroxy-3,5 dichloro or 2-hydroxy-3,5 difluoro.

Embodiment 2

[0015] Example 2 Determination of the insecticidal activity of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole

[0016] 1. Purpose of the test: To determine the toxicity of 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole to Vicia faba aphid at the test concentration in the room Evaluation of its insecticidal activity.

[0017] 2 test conditions

[0018] 2.1 Test target: broad bean aphid (Aphis fabae) is a sensitive strain that has been raised indoors with broad bean seedlings for many years, and the test insects are 3-day-old nymphs.

[0019] 2.2 Culture conditions: The culture conditions of the test target and the test target are temperature 25±5°C, relative humidity 65±5%, and light cycle 12 / 12h (L / D).

[0020] 2.3 Instruments and equipment: electronic balance (sensitivity 1 / 10,000), 100ml beaker, measuring cylinder, petri dish, paramembrane, sponge, filter paper, pipette, tweezers, brush, etc.

[0021] 3 Experimental design

[0022] 3.1 Preferred compoun...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

No PUM Login to view more

Abstract

The invention discloses application of 4-tertiary butyl-5-(1,2,4-triazole-1-base)-2-benzyliminothiazole as shown in a chemical structural formula I in the preparation of insecticides, wherein X in the chemical structural formula I is selected from hydrogen, 2-chlorine, 2-fluorine, 2-hydroxy, 2-methoxyl, 2-ethyoxyl, 2-nitryl, 3-dimethylamino, 3-chlorine, 3-bromine, 3-fluorine, 3-methyl, 3-ethyl, 3-trifluoromethyl, 3-hydroxy, 3-methoxyl, 3-ethyoxyl, 3-nitryl, 3-sulfonic group, 3-methanesulfonylamino, 3-sulfamoyl, 4-dimethylamino, 4-chlorine, 4-bromine, 4-fluorine, 4-methyl, 4-ethyl, 4-trifluoromethyl, 4-hydroxy, 4-methoxyl, 4-ethyoxyl, 4-acetoxyl group, 4-nitryl, 4-sulfonic group, 4-methanesulfonylamino, 4-sulfamoyl, 2-chlorine-5-nitryl, 3-ethyl-4-hydroxy, 3,4-dimethoxy, 2,4-dichloro, 2-hydroxy-5-bromine, 2-hydroxy-5-iodine, 2-hydroxy-5-chlorine, 2,4-difluoro, 2-hydroxy-3,5 dibromo, 2-hydroxy-3,5 diiodo, 2-hydroxy-3,5 dichloro or 2-hydroxy-3,5 difluoro.

Description

technical field [0001] The present invention relates to the application of a class of compounds in the preparation of insecticides, specifically 4-tert-butyl-5-(1,2,4-triazol-1-yl)-2-benziminothiazole in the preparation of insecticides application in agents. Background technique [0002] Azole heterocyclic derivatives have always been paid attention to by drug and pesticide workers because of their good biological activity, high drug efficacy, wide bactericidal spectrum, and good systemic property [Comperhensive Heterocylie Chemistry. Pergamon Oxford, 1983, 5: 733-735], and triazoles are one of the more influential ones. The bactericidal mechanism of triazole fungicides is to affect the formation of fungal cell walls by hindering the biosynthesis of fungal ergosterol, and have good control effects on most fungal diseases that endanger crop growth. Triazole fungicides also have certain plant growth regulating activity [Pesticides, 1994, 33 (4): 19-20; J Med Chem, 1996, 39 (...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
Patent Type & Authority Patents(China)
IPC IPC(8): A01N43/78A01P7/04A01P13/00
Inventor 陈平龙姝霍素芳沈芳
Owner CHANGSHA UNIVERSITY OF SCIENCE AND TECHNOLOGY
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products

Browse by: Latest US Patents, China's latest patents, Technical Efficacy Thesaurus, Application Domain, Technology Topic.

© 2024 PatSnap. All rights reserved.Legal|Privacy policy|Modern Slavery Act Transparency Statement|Sitemap