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Alkaline bleach liquor extraction process of bamboo wood dissolving pulp

A technology of dissolving pulp and alkali extraction, applied in pulp bleaching and other directions, can solve the problems of backward bamboo dissolving pulp production equipment and technology, insignificant improvement of pulp whiteness, large waste water pollution load, etc., and achieve stable pulp brightness. , Reduce the consumption of chemicals, the effect of high removal rate

Active Publication Date: 2011-08-17
CHONGQING LEE & MAN PAPER MFG
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] However, the existing bamboo dissolving pulp production equipment and technology are relatively backward, especially the traditional three-stage bleaching of C-E-H is mainly used in the bleaching process. The wastewater pollution load generated by the bleaching process is large, and there are internationally recognized carcinogens dioxin produce
[0004] In recent years, an improved ECF bleaching process has been adopted in China. The alkali extraction process is indispensable in the ECF bleaching process. However, in the existing alkali extraction process, it is usually only a simple alkali treatment. The improvement of whiteness is not obvious, the consumption of chemicals in the chlorine dioxide bleaching process in the later stage is relatively high, and the cost of bleaching is relatively high

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0018] A kind of alkali extraction process of bamboo dissolving pulp, it comprises the following steps:

[0019] A, washing and concentrating the pulp after chlorine dioxide bleaching to a weight concentration of 8%, adding caustic soda accounting for 1.2% of the air-dried pulp weight in the tail tank of the pulp washer, adjusting the pH value to 10.5, and the air-dried pulp contains 10 % moisture;

[0020] B. The slurry after adjusting the pH value enters the medium concentration standpipe, and 3kg / admt hydrogen peroxide is added into the medium concentration standpipe, and the weight concentration of hydrogen peroxide is 35%;

[0021] C. The slurry from the medium-concentration standpipe is pumped to the medium-consistency mixer through the medium-concentration slurry, and 3kg / admt of oxygen is added into the medium-concentration mixer (the pressure of oxygen is 1.0Mpa, and the purity of oxygen is ≥93%), and mixed Uniform;

[0022] D. The slurry from the medium-concentrati...

Embodiment 2

[0025] A kind of alkali extraction process of bamboo dissolving pulp, it comprises the following steps:

[0026] A, washing and concentrating the slurry after chlorine dioxide bleaching to a weight concentration of 10%, adding caustic soda accounting for 1.4% of the air-dried pulp weight in the tail tank of the pulp washer, adjusting the pH value to 10.6, and the air-dried pulp contains 10 % moisture;

[0027] B. After the pH value is adjusted, the slurry enters the medium concentration standpipe, and 4kg / admt hydrogen peroxide is added into the medium concentration standpipe, and the weight concentration of hydrogen peroxide is 35%;

[0028] C. The slurry from the medium concentration standpipe is pumped to the medium concentration mixer through the medium concentration slurry, and 4kg / admt of oxygen is added into the medium concentration mixer (the pressure of oxygen is 1.1Mpa, and the purity of oxygen is ≥93%), mix Uniform;

[0029] D. The slurry from the medium-concentra...

Embodiment 3

[0032] A kind of alkali extraction process of bamboo dissolving pulp, it comprises the following steps:

[0033] A, washing and concentrating the slurry after chlorine dioxide bleaching to a weight concentration of 11%, adding caustic soda accounting for 1.6% of the air-dried pulp weight in the tail tank of the pulp washer, adjusting the pH value to 10.8, and the air-dried pulp contains 10 % moisture;

[0034] B. After the pH value is adjusted, the slurry enters the medium concentration standpipe, and 4kg / admt hydrogen peroxide is added into the medium concentration standpipe, and the weight concentration of hydrogen peroxide is 35%;

[0035] C. The slurry from the medium concentration standpipe is pumped to the medium concentration mixer through the medium concentration slurry, and 4kg / admt of oxygen is added into the medium concentration mixer (the pressure of oxygen is 1.1Mpa, and the purity of oxygen is ≥93%), mix Uniform;

[0036] D. The slurry from the medium-concentra...

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PUM

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Abstract

The invention belongs to the technical field of the preparation of dissolving pulp, in particular to an alkaline bleach liquor extraction process of bamboo wood dissolving pulp, which comprises the following steps: A. washing and concentrating pulp bleached by chlorine dioxide, adding 1.2-1.8% of caustic soda, and adjusting the pH value of the pulp to be 10.5-11.0; B. after adjusting the pH value, feeding the pulp into a medium-concentrated stand tube, and adding 3-5kg / admt hydrogen peroxide; C. sending the pulp from the medium-concentrated stand tube into a medium-concentrated mixing device, and adding 3-5kg / admt of oxygen; D. sending the pulp from the medium-concentrated mixing device into an upflow tower, and then overflowing into a downflow tower, and the retention time of the pulp in the upflow tower and the downflow tower is for 75-100min, and the temperature is 80-85 DEG C; and E, pumping the pulp from the downflow tower to a pulp washing machine to wash and concentrate for standby. The alkaline bleach liquor extraction process disclosed by the invention has the advantages that the removal rate of residual lignin is high, the whiteness of the produced pulp is stable, the consumption of chemicals at a subsequent chlorine dioxide bleaching stage can be reduced, and the alpha-cellulose content in the pulp is improved.

Description

technical field [0001] The invention belongs to the technical field of preparation of dissolving pulp, in particular to an alkali extraction process of bamboo dissolving pulp. Background technique [0002] Dissolving pulp is widely used in textile viscose fiber, nitrocellulose, cellulose acetate and other cellulose derivative industries, and the market demand is gradually expanding. At present, the newly developed bamboo dissolving pulp has a broad market prospect and can fill the gap of dissolving pulp in my country. [0003] However, the existing bamboo dissolving pulp production equipment and technology are relatively backward, especially the traditional three-stage bleaching of C-E-H is mainly used in the bleaching process. The wastewater pollution load generated by the bleaching process is large, and there are internationally recognized carcinogens dioxin produce. [0004] In recent years, an improved ECF bleaching process has been adopted in China. The alkali extract...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D21C9/14D21C9/16
Inventor 李文俊
Owner CHONGQING LEE & MAN PAPER MFG
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