Quality detection method for Ruyi Zhenbao preparation

Abstract

The invention discloses a quality detection method related to a Ruyi Zhenbao preparation. The method comprises a qualitative identification method for banksia rose, dalbergia wood, clove, long pepper, safflower, cassia seeds and gallic acid and a content determination method for safflower yellow A in safflower, piperine in long pepper and cholic acid in bezoar. According to tests and research, when a sample is tested by using the identification method in the quality detection method provided in the invention, spots appear at positions on a chromatogram of the tested sample corresponding to positions where spots with same colors appear on a chromatogram of a contrast sample; negative controls produce no interference; the identification method is simple, feasible and remarkably characteristic. When the content determination method in the invention is used for determining the content of hydroxysafflower yellow A, piperine and cholic acid in the Ruyi Zhenbao preparation, it is proved thata good linear relation is obtained, that accuracy of tests of a recovery rate is high, that very good repeatability and stability are achieved and that accurate and strict control of quality of the the Ruyi Zhenbao preparation can be realized.

Description

Technical field [0001] The present invention is a drug detection method, especially the quality testing method of Ruyi Treasure Preparation. Background technique [0002] Ruyi Treasure Preparation is a traditional Tibetan experience. The prescription comes from the "Tibetan Medical Medical Recipients" by the Division Sang Jie Jiacuo. It is the first choice for Tibetan medicine to treat various neuropathy.Ruyi Treasure Maru is recorded in the national drug standard part of the local standard of Chinese medicines, standard numbers: WS 3 -BC-0314-95.130g, 60g of frankincense, 50g of yellow sunflower, beef 2g, limestone 100g, lilac 40g, Yu Ganzi 130g, black grass 40g, Gao Liang ginger 80g, 80g of woody incense, short -ear rabbit ear grass 150g, golden vermiculite 30g, hairy hairXuanzi (de -nuclear) 100g, 30g of grass fruit, 330g of scent, 40g of licorice paste, Cassia seed 60g, Tibetan woody incense 80g thirty flavors, have heat clearing, wake up brains, relax the muscles, and dry ye...

AI Technical Summary

Problems solved by technology

[0003] Ruyi Treasure Maruhara standard (Standard number: WS 3 -BC-0314-95) The quality inspection method only has microscopic identification, no identification of medicinal materials and content determination items, which cannot fully reflect the quality of the drug, and the technical content is low, and the product quality cannot be effectively controlled.

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