Dielectric-adjustable low-temperature co-firing ceramic material and preparation method thereof
A ceramic powder and dielectric technology, which is applied in the field of preparation of composite microwave ceramic materials and low-temperature co-fired ceramic devices, can solve the problem of low dielectric constant, achieve low cost, environmental protection, non-toxic side effects, and simple preparation process Effect
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[0033] Ba 1-x Sr x TiO 3 -AMoO 4 Preparation of (A=Ba, Sr or Ca) Low Temperature Co-fired Ceramics
[0034] Table 1
[0035]
[0036]
[0037] Take by weighing Ba respectively according to the component distribution ratio in each embodiment in table 1 1-x Sr x TiO 3 (x=0.4~0.6) Powder, AMoO 4 (A=Ba, Sr, Ca) powder and yB 2 o 3 ·zLi 2 O powder, add zirconia balls and absolute ethanol or water, ball mill for 20 to 24 hours, discharge, dry and grind into powder, pass through a 200-mesh sieve to obtain the required low-temperature co-fired ceramic material.
[0038] According to the traditional electronic ceramics preparation process, 8% polyvinyl alcohol (PVA) is used as a binder for granulation, and the granulated low-temperature co-fired ceramic material is dry-pressed into diameters under a pressure of 10 MPa. Green sheet, after debonding treatment at 550°C, the sample is sintered in the air atmosphere, the sintering temperature is in the range of 900-950°C, ...
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