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Fluid bed reactor

A reactor system, heater technology, applied in gaseous chemical plating, semiconductor/solid-state device manufacturing, coating, etc., can solve problems such as fluidized bed pollution

Active Publication Date: 2012-10-03
SHAANXI NON FERROUS TIAN HONG REC SILICON MATERIAL CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Another common problem is contamination of the fluidized bed at high operating temperatures due to the materials used to construct the reactor

Method used

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  • Fluid bed reactor
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Embodiment Construction

[0026] Disclosed herein is a fluidized bed for forming polycrystalline silicon by pyrolysis of a silicon-containing gas and deposition of silicon onto fluidized silicon particles or other seed particles (e.g., silicon dioxide, graphite, or quartz particles) Reactor system. A method for operating a fluidized bed reactor system is also disclosed.

[0027] Silicon is deposited on the particles in the reactor by decomposition of a silicon-containing gas selected from: silane (SiH 4 ), disilane (Si 2 h 6 ), advanced silanes (Si n h 2n+2 ), dichlorosilane (SiH 2 Cl 2 ), trichlorosilane (SiHCl 3 ), silicon tetrachloride (SiCl 4 ), dibromosilane (SiH 2 Br 2 ), tribromosilane (SiHBr 3 ), silicon tetrabromide (SiBr 4 ), diiodosilane (SiH 2 I 2 ), triiodosilane (SiHI 3 ), silicon tetraiodide (SiI 4 ), and mixtures thereof. Silicon-containing gases may be mixed with one or more halogen-containing gases, defined as any of the following: Chlorine (Cl 2 ), hydrogen chloride...

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Abstract

Fluidized bed reactor systems for producing high purity silicon-coated particles are disclosed. A vessel has an outer wall, an insulation layer inwardly of the outer wall, at least one heater positioned inwardly of the insulation layer, a removable concentric liner inwardly of the heater, a central inlet nozzle, a plurality of fluidization nozzles, at least one cooling gas nozzle, and at least one product outlet. The system may include a removable concentric sleeve inwardly of the liner. In particular systems the central inlet nozzle is configured to produce a primary gas vertical plume centrally in the reactor chamber to minimize silicon deposition on reactor surfaces.

Description

[0001] Cross References to Related Applications [0002] This application claims the benefit of US Provisional Application 61 / 262,401, filed November 18, 2009, which is hereby incorporated by reference. technical field [0003] The present disclosure relates to the pyrolysis of a silicon-containing gas in a fluidized bed to produce silicon-coated particles. Background technique [0004] Pyrolysis of silicon-containing gases in a fluidized bed is an attractive process for the production of polysilicon for the photovoltaic and semiconductor industries due to excellent mass and heat transfer, increased deposition surface, and continuous production. Fluidized bed reactors provide much higher throughputs at a fraction of the energy consumption compared to Siemens type reactors. Fluidized bed reactors can be continuous and highly automated, significantly reducing labor costs. [0005] A common problem in fluidized bed reactors is fouling around the nozzles and reactor walls bec...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C16/442C23C16/44
CPCC23C16/45576C23C16/4417H01L21/02532C23C16/24C23C16/4404H01L21/0262C23C16/442Y10S118/05
Inventor E·韦恩·奥斯本迈克尔·V·斯潘格勒莱维·C·艾伦罗伯特·J·格尔特森保尔·E·埃格沃尔特·J·施图平杰拉尔德·蔡因格尔
Owner SHAANXI NON FERROUS TIAN HONG REC SILICON MATERIAL CO LTD