New compound and extraction method and application thereof
A compound and extraction technology, applied in steroids, medical preparations containing active ingredients, organic chemistry, etc., can solve problems such as insufficient research
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Embodiment 1
[0120] Example 1 : Extraction of the compound of the present invention
[0121] A. Pretreatment of Pandanus raw materials
[0122] The pandanus raw medicinal material was dried at a temperature of 70°C for 0.8 hours, and the water content of the pandanus raw medicinal material was 0.45%, and then the dried pandanus was crushed to -60 mesh crushed to obtain Pandanus powder;
[0123] B. Extraction
[0124] In the pilot-scale multifunctional extraction tank produced by Hunan Hengyang Pharmaceutical Equipment Factory, the pandanus powder obtained in step A) is heated in steam with 90% ethanol aqueous solution according to the weight ratio of the pandanus powder to the ethanol aqueous solution of 1.0:10 Extract under reflux for 1.0 hour, after filtration, repeat the extraction of the residue 3 times, combine all the obtained extracts, concentrate under reduced pressure, and dry to obtain a dry extract;
[0125] C. Extraction
[0126] Add water to the dry extract according to ...
Embodiment 2
[0144] Example 2 : Extraction of the compound of the present invention
[0145] Proceed in the same manner as in Example 1, except that 85% aqueous ethanol is used for extraction, and dichloromethane is used as the extractant at a temperature of 90°C. Other conditions are the same as in Example 1, and the product of the present invention is also obtained.
Embodiment 3
[0146] Example 3 : Extraction of the compound of the present invention
[0147] Proceed in the same manner as in Example 1, except that 95% aqueous ethanol is used for extraction, and ethyl acetate is used as the extractant at a temperature of 75°C. Other conditions are the same as in Example 1, and the product of the present invention is also obtained.
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