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1127results about How to "Simple extraction method" patented technology

Agent for phytoremediation of soil polluted by heavy metals using the waste active Sludge as the original material and the method of the phytoremediation of soil polluted by heavy metals

Provided is a heavy metal pollution soil repairing agent using excess activated sludge as the rawmaterial, a method of extraction and a method for repairing the heavy metal pollution soil, which relates to a heavy metal pollution soil repairing agent and a method thereof and a method for repairing the heavy metal pollution soil, and solves the problems of high cost, easily secondary pollution and complex operation existing in the repair of the heavy metal pollution soil. The heavy metal pollution soil repairing agent is composed of amylose, protein, nucleic acid, phosphoric acid, amino acid, humic acid compound, uronic acid and the organic substance required for cell lifecycle. The method for distilling the heavy metal pollution soil repairing agent is as follows: the wastewater treatment excess activated sludge reacts under the condition of 80-120 KPa and 60-100 DEG for 8-20 minutes; then centrifuges for 8-20 min at the rotating speed of 5000-7000r/min. The invention adopts the home position repairing or the heterotopia repairing to repair the heavy metal pollution. The invention has low cost and no secondary pollution, simple operation, short repairing period, strong activity and wide range of application.
Owner:HARBIN INST OF TECH

Method for extracting natural Chinese medicinal herb fragrance component and application of extract thereof

The invention relates to a method for extracting a natural Chinese medicinal herb fragrance component and application of an extract thereof. The extracting method comprises the following steps: using natural Chinese medicinal herbs such as indigowoad root, fig, couch grass root and the like as main raw materials; and extracting a final black brown liquid with light sweet fragrance through the steps of mixing, primary extracting, condensing and reheating, wherein the extract is dissolved by 60 percent ethanol and then sprayed to tobacco shreds by adopting an atomizing mode to be coiled into cigarette, and the product has obvious fragrance in the cigarette. According to different physicochemical properties of substances to be extracted, the substances are extracted by using mixed solvents with different concentrations through a microwave method; therefore, the extracting and heating time is shortened, the energy is saved, the extraction efficiency and the yield are improved, and the effective components in the raw materials are obtained; a plurality of new fragrant substances such as pyrazine, pyrrole, furan and the like are produced during the reaction, so the fragrance increasing effect is more remarkable; and the extracting method is simple, the equipment is easy to operate, and the method has no pollution to the environment.
Owner:上海华宝孔雀香精有限公司

Method and system for denitrifying low-carbon high-nitrogen sewage by utilizing plant carbon source-enhanced artificial wetland

The invention discloses a method and a system for denitrifying low-carbon high-nitrogen sewage by utilizing a plant carbon source-enhanced artificial wetland. The method comprises the following steps: hydrolyzing by taking waste crops or wetland plant straws as carbon sources, and charging hydrolysate into an artificial wetland so as to improve the denitrification efficiency of the low-carbon high-nitrogen sewage. The invention simultaneously provides a treatment system, which is simple in structure, and scientific and reasonable in carbon source charging mode, and the denitrification effect of the low-carbon high-nitrogen sewage can be well realized by enhancing the artificial wetland through utilizing the plant carbon source. According to the method, the adopted plant carbon sources are cheap and easily available, the carbon release capability is strong, the bio-denitrification effect is good, and the hydrolysate is simple and practical to prepare, the carbon source charging mode is strong in continuous running capability, and the method is simple to maintain, less in secondary pollution, low in production cost, and capable of solving the technical difficulty of treating tail water in a sewage treatment plant with low carbon nitrogen ratio through artificial wetland by utilizing a simple method.
Owner:JINAN UNIVERSITY

Method for extracting pectin from orange peel and shaddock peel

The invention discloses a method for extracting pectin from orange peel and shaddock peel, which relates to the technical field of biochemical pharmacy. A technical scheme provided in the invention is as follows: the method for extracting pectin from orange peel and shaddock peel comprises the successive steps of cleaning leftovers of orange peel and shaddock peel, crushing the leftovers of orange peel and shaddock peel into particles with a particle size of 2 to 3 mm, treating the obtained particles with steam or boiling water for 5 to 8 min to passivate the activity of pectase, steeping the particles in clear water for 30 min, heating an obtained mixture to a temperature of 90 DEG C for 5 min, carrying out rinsing with clear water several times to remove bitter, pigments and soluble impurities, and after the above-mentioned pre-treatment, carrying out mixing and homogenizing, press filtration, ultrafiltration, nanofiltration I, nanofiltration II, stirring for pectin formation, press filtration, distillation and recycling, spray drying and crushing so as to prepare a pure product. Compared with the prior art, the invention has the following striking substantive advantages and remarkable progress: usage of traditional extraction methods and harmful organic solvents is reduced, original biological activity is retained during the process of extraction, the extraction process is simple and environment-friendly, and the method costs little and is applicable to large scale industrial production.
Owner:吕维学

Hyperspectral image spectral-spatial cooperative classification method based on SAE depth network

The invention relates to a hyperspectral image spectral-spatial cooperative classification method based on an SAE depth network. According to the hyperspectral image spectral-spatial cooperative classification method based on the SAE depth network, the conventional method that neighborhood information is applied to act as spatial features after PCA dimension reduction, spatial position information, i.e. row and column coordinates, of current pixel points are applied to act as the spatial features and then the spatial features are combined with spectral features to act as the spectral-spatial cooperative features of training samples can be substituted. The beneficial effects of the hyperspectral image spectral-spatial cooperative classification method based on the SAE depth network are that the conventional method of spatial feature extraction in spectral-spatial cooperative classification based on the SAE depth network is improved, the spatial position information is applied to act as the spatial features rather than the conventional method of spatial feature extraction that principal component analysis (PCA) dimension reduction is performed in spectral space and then neighborhood space information is extracted to act as the spatial features, the extraction method of the spatial features is simplified, computational burden is reduced and classification accuracy is enhanced in comparison with that of the conventional method.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Method for preparing phosphatidylserine and phosphatidylcholine

The invention relates to a method for preparing phosphatidylserine and phosphatidylcholine, and belongs to the field of food health-care products. The method comprises the following steps of: extracting soybean meal phospholipid which is used as a raw material by an organic solvent, and then distilling and drying to respectively obtain a phosphatidylcholine crude product and a phosphatidylserine crude product; and separating and purifying the phosphatidylcholine crude product and the phosphatidylserine crude product through a silica gel column of 200-300 meshes, eluting with a mixed organic solvent, concentrating the eluant, and drying to obtain phosphatidylserine and phosphatidylcholine. According to the method, the purities of the phosphatidylserine and the phosphatidylcholine meet requirements of new resource foods, so that the phosphatidylserine and the phosphatidylcholine can be used as new resource dietary supplements and have high economic added values; and the phosphatidylserine and the phosphatidylcholine are prepared at the same time by effectively combining simple extraction of the phosphatidylserine and the simple extraction of the phosphatidylcholine. By the method, the production time is shortened, the production cost is reduced, the production rate is improved, the operation is simple, and the products have safety.
Owner:成都圆大生物科技有限公司

Method for extracting rubidium salt from brine, and method for extracting cesium salt from brine

The invention discloses a method for extracting a cesium salt from brine. The cesium salt extraction method comprises the following steps: mixing the brine with an adsorbent, taking out the adsorbent after complete adsorption, and desorbing the adsorbent by adopting a desorption agent to obtain a first pregnant solution; carrying out evaporative concentration on the first pregnant solution, carrying out cooling crystallization, and separating to obtain a first crystal solid and a second pregnant solution; and adjusting the alkalinity of the second pregnant solution, carrying out fractioning extraction, separating to obtain a loaded organic phase and a raffinate, stripping the loaded organic phase by using a stripping agent to obtain a stripping solution which is a cesium salt solution. The invention also discloses a method for extracting a rubidium salt. Compared with traditional methods for extracting the rubidium salt and the cesium salt from the brine, the methods disclosed in the invention adopting adsorption enrichment, fractioning extraction and stripping to obtain the cesium salt solution and a rubidium salt solution have the advantages of simple process, effective extraction and separation of the rubidium salt and the cesium salt, and prevention of the loss of the rubidium salt and the cesium salt.
Owner:ZHENGZHOU MINERALS COMPOSITIVE UTILIZATION RES INST CHINESE GEOLOGICAL ACAD

Spirulina phatensis polysaccharide and extraction method thereof

The invention relates to spirulina phatensis polysaccharide and an extraction method thereof. The extraction method comprises the following steps of: immersing spirulina which is taken as a raw material at room temperature for seven days by using industrial ethanol, pouring ethanol, airing solid, carrying out extraction for many times by using boiling water, dialyzing fluid water for two days, after concentrating intra-dialysate, centrifuging, adding a trichloroacetic acid solution to eliminate protein, neutralizing by adding an NAOH solution till the pH value is 6.5-7.5, after dialyzing and concentrating fluid water, centrifuging, adding triploid product of industrial ethanol into supernate, standing for one night, centrifugally collecting precipitation, and drying after washing through absolute ethyl alcohol and acetone respectively so as to obtain crude aqueous extraction spirulina phatensis polysaccharide; and carrying out solid residue alkali extraction to obtain crude alkali extraction spirulina phatensis polysaccharide, and separating and eluting crude polysaccharide so as to obtain pure polysaccharide. The chemical structure of the spirulina phatensis polysaccharide is characterized in that a main chain is composed of 1,4-connection alpha-D-glucose; average every eight main chain residues have one branch; substitution is at the sixth position of a branch point; and the branch is composed of one or two 1.6 connection glucose. The extraction method of the spirulina phatensis polysaccharide disclosed by the invention is simple and convenient and has good reproducibility.
Owner:YUNNAN PHYTOPHARML +1

Gas chromatography for detection of phosphate fire-retardant plasticizer in textile

The invention discloses a gas chromatography for detection of a phosphate fire-retardant plasticizer in a textile. The gas chromatography comprises the following steps of 1, preparing a test sample solution which is supernatant, 2, preparing a gradient standard solution having the concentration of 1 to 10 micrograms per milliliter by dissolving at least one phosphate fire-retardant plasticizer in a solvent, 3, injecting the gradient standard solution into a gas chromatograph, carrying out detection by a flame photometric detector to determinate peak positions of the at least one phosphate fire-retardant plasticizer, recording corresponding peak areas, and making a standard curvilinear equation by concentrations as horizontal coordinates and the peak areas as vertical coordinates, and 4, replacing the gradient standard solution used in the step 3 with the supernatant obtained by the step 1, detecting the at least one phosphate fire-retardant plasticizer in the test sample solution and the peak areas of the at least one phosphate fire-retardant plasticizer according to the step 3, and carrying out calculation by the standard curvilinear equation obtained by the step 3 to obtain the content of the at least one phosphate fire-retardant plasticizer in the test sample solution.
Owner:THE INSPECTION & QUARANTINE TECH CENT ZHEJIANG ENTRY EXIT INSPECTION & QUARANTINE BUREAU

Method for detecting pear endogenous hormone by using ultra-high performance liquid chromatography electrospray tandem mass spectrum

The invention discloses a method for detecting a pear endogenous hormone by using an ultra-high performance liquid chromatography electrospray tandem mass spectrum. The method comprises the following steps of: crushing obtained pear tissues, then adding an extracting solution for extraction, after ending extraction, adding an extraction reagent to a system, and extracting to obtain a crude extract of the endogenous hormone; separating and purifying the crude extract by using a solid-phase extraction column to obtain a detection sample; analyzing a detection sample by using the ultra-high performance liquid chromatography electrospray tandem mass spectrum to obtain the variety and the content of the endogenous hormone in the pear tissues, wherein the extracting solution comprises isopropanol, water and hydrochloric acid, and the volume ratio of the isopropanol, the water and the hydrochloric acid is (1.5-2.5):1:(0.001-0.002), and the extraction agent is dichloromethane. The method has the advantages of high sensitivity, simple pretreatment, high recovery rate, high degree of accuracy and degree of precision and the like and is used for detecting and confirming the endogenous hormones in multiple plant issues.
Owner:ZHEJIANG UNIV
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