Broad spectrum heavy metal activity deactivator preparation method
A technology of heavy metal and passivation agent, applied in the preparation of arsenic, cadmium, chromium combined inhibitor, heavy metal mercury, lead field, can solve the problems of small scope of application, lack of fixed passivation ability, etc., to achieve wide application scope and reduce health Risk, wide-ranging effects
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Embodiment 1
[0025] A preparation method of broad-spectrum heavy metal active passivator, it comprises the following steps:
[0026] (A) Take peat rich in humic acid, decomposed compost or forest soil humus layer to remove grass roots, gravel and other impurities, and pass through a 0.5cm sieve for later use;
[0027] (B) Add 0.01 mol / L HCl or HNO to the above humic acid-rich material at a volume ratio of 1:1 3 Soak for 24 hours, fully stir twice during soaking, soak to remove fulvic acid and soluble simple organic matter in the material, this part of simple organic matter can reduce the effect of passivating agent, and can also reduce the content of impurities such as heavy metals;
[0028] (C) Filter the soaked material with a bamboo drying pad, wash it with water for 3 times, spread it out and air-dry it until the water content is less than 5%;
[0029] (D) Add 2% ZnSO% to the material obtained in step (C) in sequence 4 ·7H 2O, 10% sodium silicate and 0.10% sodium selenite, every tim...
Embodiment 2
[0032] A preparation method of broad-spectrum heavy metal active passivator, it comprises the following steps:
[0033] (A) Take peat rich in humic acid, decomposed compost or forest soil humus layer to remove impurities such as grass roots and gravel, and pass through a 1cm sieve for later use;
[0034] (B) Add 0.05 mol / L HCl or HNO to the above humic acid-rich material at a volume ratio of 1:1 3 Soak for 20 hours, fully stir 3 times during soaking, soak to remove fulvic acid and soluble simple organic matter in the material, this part of simple organic matter can reduce the effect of passivating agent, and can also reduce the content of impurities such as heavy metals;
[0035] (C) Filter the soaked material with a bamboo drying pad, wash it with water for 3 times, spread it out and air-dry it until the water content is less than 5%;
[0036] (D) Add 4% ZnSO% to the material obtained in step (C) in sequence 4 ·7H 2 O, 6% sodium silicate and 0.10% sodium selenite, every ti...
Embodiment 3
[0039] A preparation method of broad-spectrum heavy metal active passivator, it comprises the following steps:
[0040] (A) Take peat rich in humic acid, decomposed compost or forest soil humus layer to remove impurities such as grass roots and gravel, and pass through a 0.8cm sieve for later use;
[0041] (B) Add 0.03 mol / L HCl or HNO to the above humic acid-rich material at a volume ratio of 1:1 3 Soak for 22 hours, fully stir twice during soaking, soak to remove fulvic acid and soluble simple organic matter in the material, this part of simple organic matter can reduce the effect of passivating agent, and can also reduce the content of impurities such as heavy metals;
[0042] (C) Filter the soaked material with a bamboo drying pad, wash it with water for 3 times, spread it out and air-dry it until the water content is less than 5%;
[0043] (D) Add 3% ZnSO% to the material obtained in step (C) in sequence 4 ·7H 2 O, 8% sodium silicate and 0.075% sodium selenite, every t...
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