Method for producing chondroitin sulfate and realizing clean co-production of protein peptides, bone oil and bone meal
A technology of chondroitin sulfate and protein peptide, which is applied in the chemical industry, can solve the problems of large ethanol consumption, long cycle, and difficult discharge of waste water to meet the standards, and achieve significant economic and social benefits
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Embodiment 1
[0022] Select 1,000 kg of chicken leg bones, crush them into pieces below 1 cm, put them into a vacuum tank, add 800 kg of distilled water, heat with steam, control the temperature in the tank to 65°C, and vacuum to 0.01 MPa, and heat for 2 hours. Put the feed liquid into the enzymatic hydrolysis tank to adjust the pH to 7.5; add 3 kg of trypsin, 1 kg of flavor protease and 4 kg of alkaline protease, keep the temperature at 35°C, and perform enzymatic hydrolysis for 4 hours. After enzymatic hydrolysis, use a disc-type three-phase centrifuge to centrifuge and separate, and the upper layer is separated to obtain 50 kg of bone oil; after the bone residue is pulverized, 760 kg of bone powder is obtained. Concentrate the centrifuged filtrate through a three-effect concentrator. During the concentration process, control the temperature of the first effect at 90°C, the second effect at 80°C, and the third effect at 65°C. When the volume is 50% of the original filtrate, stop the concen...
Embodiment 2
[0024] Select 1,000 kg of chicken ball bones, crush them into pieces below 1 cm, put them into a vacuum tank, add 900 kg of distilled water, heat with steam, control the temperature in the tank to 70°C, vacuum degree 0.02 MPa, and heat for 2.3 hours. Put the feed liquid into the enzymatic hydrolysis tank to adjust the pH to 8.0; add 4 kg of trypsin, 2 kg of flavor protease and 5 kg of alkaline protease, keep the temperature at 38°C, and perform enzymatic hydrolysis for 5 hours. After the enzymatic hydrolysis, the disc type three-phase centrifuge was used for centrifugal separation, and the upper layer was separated to obtain 55 kg of bone oil; after the bone residue was pulverized, 746 kg of bone powder was obtained. Concentrate the centrifuged filtrate through a three-effect concentrator. During the concentration process, control the temperature of the first effect at 93°C, the second effect at 83°C, and the third effect at 68°C. When the volume is 55% of the original filtrate...
Embodiment 3
[0026] Select 1,000 kg of duck breast bones, crush them into pieces below 1 cm, put them into a vacuum tank, add 950 kg of distilled water, heat with steam, control the temperature in the tank to 80°C, and the vacuum degree to 0.03 MPa, and heat for 2.5 hours. Put the feed liquid into the enzymatic hydrolysis tank to adjust the pH to 8.0; add 5 kg of trypsin, 3 kg of flavor protease and 7 kg of alkaline protease, keep the temperature at 40°C, and perform enzymatic hydrolysis for 6 hours. After enzymatic hydrolysis, centrifuge separation with a disc-type three-phase centrifuge, and 72 kg of bone oil is obtained from the upper layer separation; 735 kg of bone powder are obtained after the bone residue is pulverized. Concentrate the centrifuged filtrate through a three-effect concentrator. During the concentration process, control the temperature of the first effect at 95°C, the second effect at 85°C, and the third effect at 70°C. When the volume is 50% of the original filtrate, s...
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