A kind of pharmaceutical composition for treating and/or preventing Alzheimer's disease and use thereof
A technology for Alzheimer's disease and composition, applied in the field of pharmaceutical composition containing galantamine
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Embodiment 1
[0026] Evaluation of the Inhibitory Activity of Galantamine and Lycorine Oxide on Acetylcholinesterase by Modified Ellman Method
[0027] Instruments and materials
[0028] Instruments: BioTek Synergy2 multifunctional microplate reader (BioTek, USA), high-speed cryogenic centrifuge (SovallEvolutionRC, Kendro Corporation), vortex shaker (Vortex-Genie2, Scientific Industries, USA).
[0029] Reagents: acetylcholinesterase (AchE, from electric eel, enzyme activity: 687U / mg protein, Mr280kDa), acetylthiocholineiodide (AchE, AchE substrate, Mr289.2); 5,5'-di Thio-dithiobis(2-nitrobenzoic acid) (5,5-dithiobis(2-nitro)benzoic acid, DTNB) were purchased from Sigma–Aldrich (St. Louis, MO, USA); ultrapure water (Millipore, USA) , Tris-Hydroxymethylaminomethane Tris-base (Biosharp, Korea), and other reagents are of analytical grade.
[0030] Preparation of solution
[0031] Tris / HCl buffer: 20mM Tris buffer, containing 100mM NaCl, pH 7.5; AChE solution: take For AChE stock solution (...
Embodiment 2
[0053] Analysis on the effect of combined administration of galantamine and lycorine oxide
[0054] Based on the Median-effect Principle (moderate effect principle), the dose-response curve and the combination index curve (Fa-C curve) under different effects were drawn by using the CombiDrug statistical software. ,3,4,5 and figure 1 ,2,3,4,5) Quantitatively evaluate the synergistic, antagonistic or additive relationship between the two drugs. Specific steps are as follows:
[0055] The effect of the drug is the inhibition rate (fa)=1-(the reaction rate of the test sample solution / the reaction rate of the blank control sample) according to the intermediate effect equation fa / fu=(D / Dm) m , take the logarithm logfa / fu=mlogD-mlogDm on both sides, set a=-mlogDm, b=m, x=logD, y=logfa / fu, and substitute into the intermediate effect equation to get y=bx-a; where fa is the drug effect , fu=1-fa, D is the drug concentration, m is the slope, and Dm is the intermediate effect concentra...
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