A method for preparing hydrogel by modifying tea residue and application of the hydrogel
A hydrogel and cellulose hydrogel technology, applied in the field of natural polymer modification technology, can solve the problems of wasting potential resources, environmental pollution, etc., and achieve the effects of easy operation, less process equipment, and improved resource utilization
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Embodiment 1
[0043] (1) One leaf of fresh green tea is steamed, dried, crushed, and sieved to obtain pretreated tea leaves;
[0044] (2) Soak the pretreated tea leaves and water at a mass ratio of 1:25, at a water temperature of 70°C, for 10 minutes each time, extract water-soluble components, filter, and dry. Use petroleum ether as a solvent, soak and stir for 1 hour to degrease, wash with water, decolorize with acetone, wash, and dry to obtain degreasing and decolorized green tea residue.
[0045](3) Mix the degreased and decolorized green tea residue with 1% NaOH solution at a material-to-liquid ratio of 1:10 (g:mL) evenly, place in a water bath at a constant temperature of 30°C for 1 hour, filter with suction, and wash with water. Then mix it with concentrated sulfuric acid according to the material-to-liquid ratio of 1:10 (g:mL), acidify at a constant temperature of 40°C for 1 hour, filter with suction, wash with water, and dry to obtain a leaf of tea dregs cellulose;
[0046] (4) Us...
Embodiment 2
[0049] (1) steam green tea two leaves, dry, crush, and sieve to obtain pretreated tea leaves;
[0050] (2) Soak the pretreated tea leaves and water at a mass ratio of 1:25, at a water temperature of 80°C, for 15 minutes each time, extract water-soluble components, filter, and dry. Use petroleum ether as a solvent, soak and stir for 1.5 hours to degrease, wash with water, decolorize with acetone, wash, and dry to obtain degreasing and decolorized green tea residue.
[0051] (3) Mix the degreased and decolorized green tea residue with 2% NaOH solution at a material-to-liquid ratio of 1:15 (g:mL) evenly, bathe in a water bath at a constant temperature of 35°C for 1.5 hours, filter with suction, and wash with water. Then mix it evenly with concentrated sulfuric acid according to the material-to-liquid ratio of 1:15 (g:mL), acidify at a constant temperature of 50°C for 1 hour, filter with suction, wash with water, and dry to obtain the two-leaf tea residue cellulose;
[0052] (4) ...
Embodiment 3
[0055] (1) Steam greening three leaves of fresh green tea, dry, crush, and sieve to obtain pretreated tea leaves;
[0056] (2) Soak the pretreated tea leaves and water at a mass ratio of 1:30 at a water temperature of 90°C for 3 times, each soaking time is 20 minutes, extract water-soluble components, filter, and dry. Use petroleum ether as a solvent, soak and stir for 1.5 hours to degrease, wash with water, decolorize with acetone, wash, and dry to obtain degreasing and decolorized green tea residue.
[0057] (3) Mix the degreased and decolorized green tea residue with 3% NaOH solution at a material-to-liquid ratio of 1:20 (g:mL) evenly, place in a water bath at a constant temperature of 40°C for 1.5 hours, filter with suction, and wash with water. Then mix it evenly with concentrated sulfuric acid according to the material-to-liquid ratio of 1:20 (g:mL), acidify at a constant temperature of 60°C for 1 hour, filter with suction, wash with water, and dry to obtain the three-le...
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