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Quality detection method for Tibetan medicine composition rheumatism Theron preparation

A technology for rheumatoid sialon solid and preparation, which is applied in the field of medicine, can solve the problems that the quality standard needs to be improved, the quality of main components cannot be effectively controlled, and the quality of this product cannot be controlled comprehensively and accurately, and the product quality is safe and the quality is acceptable. control effect

Active Publication Date: 2014-06-11
JINHE TIBETAN MEDICINE
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0005] However, the existing quality testing standards for Fengshi Sailong Capsules only use TLC to identify two medicinal materials, antler antler and woody wood, and HPLC to determine the content of one active ingredient, gallic acid, and the number of selected identification items is too small and unrepresentative property, and cannot effectively control the quality of other main components
Therefore, the existing quality detection methods cannot comprehensively and accurately control the quality of this product, and the quality standard needs to be improved.

Method used

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  • Quality detection method for Tibetan medicine composition rheumatism Theron preparation
  • Quality detection method for Tibetan medicine composition rheumatism Theron preparation
  • Quality detection method for Tibetan medicine composition rheumatism Theron preparation

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0369] Embodiment 1: the quality detection method of Fengshi Sailong Capsules

[0370] Identification:

[0371] (1) Identification of Zicao antler

[0372]Take 10g of the content of Fengshi Sialon Capsules, add 20ml of ethyl acetate, ultrasonically treat for 30 minutes, filter, and concentrate the filtrate to 2ml, and use it as the test solution; take 0.5g of the antler reference medicinal material, and prepare the reference medicinal material solution in the same way Carry out the test according to the Chinese Pharmacopoeia 2010 edition one appendix VIB thin-layer chromatography method, draw each 10 μ L of above-mentioned two kinds of solutions, point respectively on the same silica gel G thin-layer plate, with 5: 5: 0.5: 0.1 xylene-dichloromethane -Acetone-formic acid is used as a developing agent, developed, taken out, dried, and inspected under sunlight respectively; in the chromatogram of the test product, on the position corresponding to the chromatogram of the control ...

Embodiment 2

[0405] Embodiment 2: the quality detection method of Fengshi Sialon Granules

[0406] Identification:

[0407] (1) Identification of Zicao antler

[0408]Take 10g of Rheumatism Sialon Granules, add 20ml of ethyl acetate, ultrasonically treat for 30 minutes, filter, and the filtrate is concentrated to 2ml, as the test solution; take 0.5g of antler reference medicinal material, and prepare the reference medicinal material solution in the same way; Chinese Pharmacopoeia 2010 Edition, Appendix ⅥB thin-layer chromatography test, draw 10 μL of each of the above two solutions, respectively spot on the same silica gel G thin-layer plate, with 5:5:0.5:0.1 xylene-dichloromethane-acetone - Formic acid is used as a developing agent, unfolded, taken out, dried, and inspected under sunlight respectively; in the chromatogram of the test product, on the position corresponding to the chromatogram of the control medicinal material, spots and fluorescent spots of the same color appear;

[0409...

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Abstract

The invention discloses a quality detection method for a Tibetan medicine composition rheumatism Theron preparation. With the adoption of the quality detection method, the quality standard of an existing rheumatism Theron preparation is correspondingly improved and an identification method for shellac and elecampane in a previous standard is optimized; the identification on juniperus formosana, syzygium aromaticum, meconopsis, rubia wallichiana decne and amomum kravanh is increased on the basis of the previous standard, and a content determination method of general flavone and swertia chirayita and a detection method for aristolochic acid A are increased, so as to further ensure the safe, efficient, uniform and stable product quality and the controllable quality.

Description

technical field [0001] The invention relates to a quality detection method of a Tibetan medicine composition, in particular to a quality detection method of a Tibetan medicine composition Rheumatic Theron preparation, belonging to the technical field of medicine. Background technique [0002] The term rheumatism originated in ancient Greece. In the 4th century BC, the article on human anatomy in "The Complete Works of Hippocrates" believed that: the body fluids of the human body are poured into the limbs and internal organs due to dampness and cold, causing diseases, which is rheumatism. my country's "Huangdi Neijing" also refers to the hybrid of the three phases of wind, cold and dampness as numbness. [0003] Tibetan medicine researched rheumatism earlier. Tibetan medicine believes that the gout caused by Long, Chiba, blood, and Bacon has a short and tight pulse like blood fever, slow pulse, erratic urine, and a heat syndrome. Sometimes the joints are dry and painful. D...

Claims

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Application Information

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IPC IPC(8): G01N30/90G01N21/31G01N30/02
Inventor 郑亭亭江玉娟任松鹏宋洋单玉刚
Owner JINHE TIBETAN MEDICINE
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