Preparation method of 3D printing inorganic powder molding material

A technology of inorganic powder and molding materials, applied in the field of rapid prototyping materials, can solve the problems that restrict the promotion and popularization of 3DP molding technology, the molding precision of tiny parts is not high enough, thin-walled parts are not easy to shape, etc., and achieve narrow particle size distribution range and easy The effect of industrialized production and low production cost

Inactive Publication Date: 2014-07-23
UNIV OF JINAN
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] 3D printing technologies include 3DP technology, FDM fusion lamination molding technology, SLA stereolithography technology, SLS selective laser sintering technology, DLP laser molding technology and UV ultraviolet molding technology. The most widely used is FDM3D printing technology. This technology can be used in the home. It is easy to operate and the materials used are generally available. The products printed by this technology are also close to our daily necessities. The materials used are mainly environmentally friendly polymer materials. Such as: PLA, PCL PHA PBS PA ABS PC PS POM PVC, because this technology is generally printed on the desktop, the odor produced by the molten polymer material or the harmful substances produced by decomposition directly contact with our people, which is easy to cause safe question
[0007] Due to the large particle size of the 3DP rapid prototyping material powder, it is difficult to form thin-walled parts, the forming accuracy of tiny parts is not high enough, and the surface has a relatively rough feeling; in addition, because the binder is not strong enough, there is a low strength of the formed part Not enough
In addition, the 3DP molding materials currently sold in the market are basically monopolized by foreign companies, and the price is high, which seriously restricts the promotion and popularization of 3DP molding technology in my country.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0024] (1) Aluminum powder pretreatment: Add 30mL acetone and 70g aluminum powder to the grinder, turn on the grinder at 800 rpm, grind at room temperature for 40min, then add 6g γ-(2,3-glycidyloxypropoxy ) Propyltrimethoxysilane, the rotating speed is at 800 rpm, and the grinding is continued for 1.5h at room temperature to obtain pretreated aluminum powder;

[0025] (2) Preparation of 3D printing aluminum powder molding materials: In the reactor, add 60 mL of acetone, add 5 g of polyvinyl formal, stir to dissolve, add 47 g of pretreated aluminum powder, stir to mix evenly, and put it into a grinder In the process, the rotation speed was 800 rpm, mixed and ground at room temperature for 7.5 h, and then spray-dried to obtain 3D printing aluminum powder molding materials.

Embodiment 2

[0027] (1) Aluminum powder pretreatment: Add 38mL acetone and 62g aluminum powder to the grinder, turn on the grinder at 1000 rpm, grind at room temperature for 30min, then add 8g γ-(2,3-glycidyloxypropoxy ) Propyltrimethoxysilane, the rotating speed is at 1000 rpm, and the grinding is continued for 2h at room temperature to obtain pretreated aluminum powder;

[0028] (2) Preparation of 3D printing aluminum powder molding materials: In the reactor, add 75 mL of acetone, add 8g of polyvinyl formal, stir to dissolve, add 32g of pretreated aluminum powder, stir and mix evenly, put into the grinder 3D printing aluminum powder molding material was obtained by mixing and grinding at room temperature for 9 h at a rotational speed of 1000 rpm, and then spray drying.

Embodiment 3

[0030] (1) Aluminum powder pretreatment: Add 15mL acetone to the grinder, add 80g aluminum powder, turn on the grinder at 500 rpm, grind at room temperature for 50min, then add 8g γ-(2,3-glycidyloxypropoxy ) Propyltrimethoxysilane, the rotating speed is at 500 rpm, and the grinding is continued for 1h at room temperature to obtain pretreated aluminum powder;

[0031] (2) Preparation of 3D printing aluminum powder molding materials: In the reactor, add 50 mL of acetone, add 3 g of polyvinyl formal, stir to dissolve, add 57 g of pretreated aluminum powder, stir to mix evenly, and put it into a grinder 3D printing aluminum powder molding materials were obtained by mixing and grinding at room temperature for 6 h at a rotational speed of 500 rpm, and then spray drying.

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Abstract

The invention discloses a preparation method of a 3D printing inorganic powder molding material. The method is characterized in that the method comprises the following steps: 1, powder material pretreatment: mixing 10-30% of acetone with 62-85% of a powdery material and 2-10% of gamma-(2,3-epoxypropoxy)propyltrimethoxysilicane, and grinding the obtained mixture at a rotating speed of 500-1000rpm for 1-2h to obtain a pretreated powdery material; and 2, molding material preparation: adding 40-65% by mass of acetone, adding 2-8% of polyvinyl formal, stirring for dissolving, adding 30-55% of the pretreated powdery material, stirring for uniform mixing, putting the obtained solution in a grinder, carrying out normal temperature mixing grinding at a rotating speed of 500-1000rpm for 6-9h, and carrying out spray drying to obtain the 3D printing inorganic powder molding material. The 3D printing inorganic powder molding material can be directly molded at a temperature of 190-210DEG C under a pressure of 1-10MPa without sprinkling a binder, and has the advantages of simple preparation technology, easy condition control, low production cost and easy industrialized production.

Description

technical field [0001] The invention relates to a method for preparing 3D printing inorganic powder molding materials, which belongs to the field of rapid prototyping materials, and in particular to a preparation process for 3D printing rapid prototyping inorganic powder materials. Background technique [0002] Rapid Prototyping Technology, also known as Rapid Prototyping Manufacturing (RPM) technology, was born in the late 1980s. It is a high-tech manufacturing technology based on the material accumulation method and is considered to be a major achievement in the manufacturing field in recent years. It integrates mechanical engineering, CAD, reverse engineering technology, layered manufacturing technology, numerical control technology, material science, and laser technology, and can automatically, directly, quickly and accurately transform design ideas into prototypes with certain functions or directly manufacture parts , so as to provide a high-efficiency and low-cost real...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B33/13C04B35/63C03C3/06B22F1/00B22F9/04
Inventor 李慧芝张培志许崇娟
Owner UNIV OF JINAN
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