Photosensitive Resin Composition For Black Matrix, Black Matrix, Optical Filter And Display
A technology of photosensitive resin and black matrix, applied in the field of photosensitive resin composition, can solve the problem of low surface resistance value
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[0176] Preparation method of photosensitive resin composition for black matrix
[0177] The method that can be used to prepare photosensitive resin composition for black matrix is for example: with alkali-soluble resin (A), compound (B) with ethylenically unsaturated group, photoinitiator (C), solvent (D), black pigment ( E), the first crosslinking agent (F) and inorganic particles (G) are placed in a stirrer and stirred to make them uniformly mixed into a solution state. Additives (H) can also be added if necessary. After uniformly mixed, you can obtain A photosensitive resin composition for a black matrix in a solution state.
[0178] Moreover, the preparation method of the photosensitive resin composition for black matrices is not specifically limited. The black pigment (E) can be directly added to the alkali-soluble resin (A), a compound (B) having an ethylenically unsaturated group, a photoinitiator (C), a solvent (D), a first crosslinking agent (F) and It is formed b...
Synthetic example A-1
[0201] Synthesis Example A-1-1 to Synthesis Example A-1-3 of the resin (A-1) having an unsaturated group are described below:
Synthetic example A-1-1
[0203] First, 100 parts by weight of fluorene epoxy compound (model ESF-300, manufactured by Nippon Steel Chemical; epoxy equivalent 231), 30 parts by weight of acrylic acid, 0.3 parts by weight of benzyltriethylammonium chloride, 0.1 parts by weight of Parts of 2,6-di-tert-butyl-p-cresol and 130 parts by weight of propylene glycol methyl ether acetate were added to a 500 ml four-neck flask in a continuous manner. The feed rate is controlled at 25 parts by weight / min, and the temperature during the reaction is maintained at 100°C to 110°C. After 15 hours of reaction, a light yellow transparent mixed liquid with a solid content concentration of 50wt% can be obtained.
[0204] Then, 100 parts by weight of the above-mentioned light yellow transparent mixed solution was dissolved in 25 parts by weight of ethylene glycol ether acetate, and simultaneously added 6 parts by weight of tetrahydrophthalic anhydride and 13 parts by weight of diphenyl Methanone tetracarboxylic dianhydride....
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