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A method for extracting natural pigment from fruit shell

A natural pigment and fruit shell technology, applied in natural dyes, chemical instruments and methods, azo dyes, etc., can solve the problems of difficult post-processing, low impurity content, and low extraction rate

Active Publication Date: 2016-06-15
杭州俐生美健康科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Aiming at the existing problems of low extraction rate, large impurity content, difficult post-processing, high impurity content, etc., the present invention proposes a method for extracting natural pigments from fruit shells. The method has high extraction rate, simple post-processing and low impurity content. Low

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0019] Pick out the chestnut shells without mildew, put them in an oven at 70°C, dry them, and crush them with a jet mill. The powder is a mixture of chestnut shell red coat and inner membrane; weigh 20g of chestnut shell powder, add 400mL of 50% Phosphate buffer solution, leaching in a water bath at 60°C for 2 hours, after cooling, filter, centrifuge, and suction filter the extract; add 350mL of 60% phosphate buffer solution to the above chestnut shell powder, and then add 10mg / g of acid-base The fibers were enzymolyzed in a water bath at 40°C for 100 minutes, and then heated in a water bath at 90°C for 5 minutes to inactivate the enzyme; put the above-mentioned mixed solution after inactivating the enzyme into a 500W ultrasonic wave, and the temperature was controlled at 50°C. The ultrasonic treatment time is 15 minutes; the ultrasonic extract is cooled, filtered and centrifuged, vacuum concentrated to a certain concentration with a rotary evaporator, and then subjected to hi...

example 2

[0021] Pick out the chestnut shells without mildew, put them in an oven at 70°C, dry them, and crush them with a jet mill. The powder is a mixture of chestnut shell red coat and inner membrane; weigh 20g of chestnut shell powder, add 400mL of 50% Phosphate buffer solution, leaching in a water bath at 60°C for 2 hours, after cooling, filter, centrifuge, and suction filter the extract; add 350mL of 60% phosphate buffer solution to the above-mentioned chestnut shell powder, and then add 11mg / g of acid-base The fibers were enzymolyzed in a water bath at 45°C for 110 minutes, and then heated in a water bath at 90°C for 5 minutes to inactivate the enzyme; put the above-mentioned mixed solution after inactivating the enzyme into a 550W ultrasonic wave, and the temperature was controlled at 50°C. The ultrasonic treatment time is 18 minutes; the ultrasonic extract is cooled, filtered and centrifuged, vacuum concentrated to a certain concentration with a rotary evaporator, and then subje...

example 3

[0023] Pick out the chestnut shells without mildew, put them in an oven at 70°C, dry them, and crush them with a jet mill. The powder is a mixture of chestnut shell red coat and inner membrane; weigh 20g of chestnut shell powder, add 400mL of 50% Phosphate buffer solution, leaching in a water bath at 60°C for 2 hours, after cooling, filter, centrifuge, and suction filter the extract; add 350mL of 60% phosphate buffer solution to the above-mentioned chestnut shell powder, and then add 12mg / g of acid-base Fibers were enzymolyzed in a water bath at 50°C for 120 minutes, and then heated in a water bath at 90°C for 5 minutes to inactivate the enzyme; put the above-mentioned mixed solution after inactivating the enzyme into a 600W ultrasonic wave, and the temperature was controlled at 50°C. The ultrasonic treatment time is 20min; the ultrasonic extract is cooled, filtered and centrifuged, vacuum concentrated to a certain concentration with a rotary evaporator, and then subjected to h...

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Abstract

The invention relates to a method for extracting a natural pigment from a fruit shell. The method for extracting the natural pigment from the fruit shell has the advantages that an ultrasonic-assisted enzyme method is adopted for extracting a brown pigment from a chestnut shell under the conditions that a phosphate buffer solution is taken as an extracting agent, the ratio of material to liquor is 1:20, the enzyme adding amount is 10-12mg / g, the enzymolysis time is 100-120 minutes, an assisted ultrasonic wave is 500-600W and the ultrasonic time is 15-20 minutes, and the extraction rate reaches up to more than 90%.

Description

technical field [0001] The invention relates to a method for extracting natural pigments, in particular to a method for extracting natural pigments from fruit shells. Background technique [0002] Food coloring, also known as food coloring agent, is an edible substance that improves the color and luster of food, and belongs to a large category of food additives. It is not only widely used in the food industry to improve the color of food and enhance people's enjoyment of beauty, but also widely used in medicine and cosmetics. Food coloring is generally divided into two categories: food natural coloring and food synthetic coloring. Synthetic plain colors were once widely used due to their advantages such as strong tinting strength, bright color, good stability, odorless and tasteless, uniform quality, easy dissolution and color matching, and low cost. However, incidents such as Sudan red and malachite green have caused round after round of food safety warnings, and people h...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C09B61/00
CPCC09B61/00
Inventor 汪巍
Owner 杭州俐生美健康科技有限公司