Synthesis method and application of low-phosphorous corrosion and scale inhibitor
A corrosion and scale inhibitor and synthesis method technology, applied in the field of water treatment, can solve problems such as environmental secondary pollution, highly toxic cyanide, complex process routes, etc., achieve the effect of low phosphorus content and reduce phosphate efflux
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[0016] Add 6.9kg diethyl phosphite and 8.6kg maleic diethyl ester in the reactor, open the condensing reflux device, be 200r / min at the stirrer speed, slowly drip under the stirring condition that the stirrer speed is 200r / min Add 2.4kg of catalyst A, and react for 1 hour after the temperature rises to 100°C. Then the temperature was lowered to 50° C., 5.0 kg of ethyl acrylate was added, and the mixture was stirred for 8 hours. Then add 8L of catalyst B into the reactor, heat up to 80° C. and heat and hydrolyze for 0.5 h. The final product obtained is 12.5 kg of yellow-brown viscous liquid, which is PBTCA of the present invention. When the circulating cooling water temperature is 40°C, the dosage is 5g / m 3 When the scale inhibition rate reaches 90.70%; the dosage is 56g / m 3 , the corrosion inhibition rate reached 81.62%, and the corrosion rate was 0.11mm / a, reaching the standard of 3 / h, at least PO can be reduced every year 4 3- The discharge volume is 50t.
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