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Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent and application of Luculia pinceana Hook.extract with glycerol triacetate serving as extracting agent to cigarettes

A technology of glyceryl triacetate and clove yunnanensis, applied in the application of glyceryl triacetate extract of clove yunnanensis in cigarettes, in the field of glyceryl triacetate extract of clove yunnanensis, can solve the difficulty of filter sticks, increase production costs, and the solubility of additives Limited, unfavorable promotion and application, etc., to achieve the effect of strong operability and standardization, good application prospects, and rich aroma

Inactive Publication Date: 2016-07-20
CHINA TOBACCO YUNNAN IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

On the one hand, this method of adding and applying has complicated preparation process and limited dissolving ability of triacetin for additives, and many extracts that have the effect of enhancing and invigorating the flavor of cigarettes are difficult to dissolve in triacetin, which limits this type of Application of Extract in Cigarette Filter Stick
On the other hand, if the filter rod is not flavored with triacetin as a carrier, but the additive is directly applied to the cigarette filter rod, it will bring greater difficulty to the production of the filter rod and significantly increase the production cost, which is not conducive to large-scale production. Scale promotion and application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0021] Take fresh lilac flowers and dry them in the sun, pulverize them with a pulverizer, pass the obtained powder through a 20-mesh sieve, weigh 300g of lilac powder in a round bottom flask, and add glycerol triacetate for tobacco at a ratio of 1:6. After soaking at room temperature for 2 hours, reflux extraction was carried out at 70°C for 4 hours, and the extraction time was 4 hours, then cooled to room temperature naturally, and the clove and glyceryl triacetate after the reflux extraction were placed in an ultrasonic extraction device (400W, 40kHZ), extract for 30 minutes, and filter to remove the filter residue to obtain a clear solution, which is the desired triacetin extract of Dian clove.

[0022] Using glyceryl triacetate as a solvent, the extract of clove triacetin is prepared into a solution with a concentration of 0.03%, and it is evenly sprayed on the filter rod tow according to the weight ratio of 7% of the acetate fiber tow to make a cigarette filter rod , thr...

Embodiment 2

[0024] Take fresh lilac flowers and dry them, grind them through a pulverizer, pass the obtained powder through a 40-mesh sieve, weigh 400g of lilac powder in a round bottom flask, and add glycerol triacetate for tobacco at a ratio of 1:8. As an extractant, after soaking at room temperature for 3 hours, carry out reflux extraction at 80°C for 5 hours, cool naturally to room temperature, and place the clove and triacetin after the reflux extraction in ultrasonic extraction equipment (500W, 40kHZ), extract for 40 minutes, filter and remove the filter residue to obtain a clear solution, and you can get the desired Dian clove triacetin extract.

[0025] Using glyceryl triacetate as a solvent, the extract of clove triacetin is prepared into a solution with a concentration of 0.04%, and evenly sprayed on the filter rod tow according to the weight of 7.5% of the acetate fiber tow to make a cigarette filter rod , through conventional cigarette tipping procedures to make cigarettes con...

Embodiment 3

[0027] Take fresh lilac flowers and dry them, pulverize them with a pulverizer, pass the obtained powder through a 30-mesh sieve, weigh 500g of lilac powder in a round bottom flask, and add glycerol triacetate for tobacco at a ratio of 1:10 As an extractant, after soaking at room temperature for 4 hours, reflux extraction was carried out at 90°C for 6 hours, and naturally cooled to room temperature, and the reflux-extracted clove and glyceryl triacetate were placed in ultrasonic extraction equipment (600W, 40kHZ), extract for 50 minutes, filter and remove the filter residue to obtain a clear solution, and you can obtain the required Dian clove triacetin extract.

[0028] Using glyceryl triacetate as a solvent, the extract of clove triacetin is formulated into a solution with a concentration of 0.05%, and is evenly sprayed on the filter rod tow in a proportion of 8% by weight of acetate fiber tow to make a cigarette filter rod. Cigarettes containing the active ingredient filter...

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PUM

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Abstract

The invention discloses a Luculia pinceana Hook.extract with glycerol triacetate serving as an extracting agent and application of the Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent to cigarettes. The Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent is prepared from ground and sieved dried flower of Luculia pinceana Hook.with the glycerol triacetate serving as the extracting agent through heating reflux extraction and then ultrasonic extraction. The Luculia pinceana Hook.extract is prepared into a 0.03-0.06% solution with the glycerol triacetate serving as a solvent, the solution is uniformly sprayed to filter stick tows according to a proportion accounting for 7-8% of the weight of cellulose acetate tows to obtain filter sticks of the cigarettes, and then a conventional cigarette tipping process is conducted so as to obtain the cigarettes with the filter sticks containing Luculia pinceana Hook. The Luculia pinceana Hook.extract can enrich the aroma of the cigarettes and enhance volatility of smoke and is clean in aftertaste so as to improve smoking comfort obviously. The Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent and application of the Luculia pinceana Hook.extract with the glycerol triacetate serving as the extracting agent to the cigarettes have the advantages of high operability and standardability, easy availability to raw materials, low cost, simple production technology, capability of achieving industrial production easily and promising application prospect.

Description

technical field [0001] The invention belongs to the technical field of cigarette materials, and in particular relates to an extract of glycerol triacetate from clove yunnanensis. At the same time, the present invention also relates to the application of the clove triacetin extract in cigarettes. Background technique [0002] Dian lilac (Luculia pinciana Hook.) is a plant of the genus Dian lilac in Rubiaceae, which is distributed from the Himalayas to Yunnan and Guangxi of my country, and has high garden and medicinal value. Due to its beautiful plant shape, luxuriant branches and leaves, bright emerald green, long flowering period, dense and luxuriant flowers, bright and fragrant flowers, it is mainly used as an ornamental flower and tree at present. But it also has a long history as a traditional Chinese medicinal material among the people. According to records: clove leaves, its taste is bitter, pungent, slightly warm in nature; fragrance enters the lungs, relieves lung-...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C11B9/00A24D3/14
CPCC11B9/0003A24D3/14
Inventor 韦克毅陈兴陈薇杨莹蔡波杨乾栩赵蔚
Owner CHINA TOBACCO YUNNAN IND
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