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Preparation method of cigarette tip rod with supramolecular controlled-release cool essence

A supramolecular and cooling technology, applied in the field of tobacco, can solve the problems of short duration of cool feeling and affect the taste of products, so as to increase the storage time, reduce the harm to human health, and prolong the release time

Inactive Publication Date: 2016-07-27
HUBEI CHINA TOBACCO IND
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

With the continuous improvement of people's requirements for cool products, the shortcomings and deficiencies of menthol are gradually exposed, which are mainly manifested in two aspects. One is in terms of high temperature resistance. , especially the loss of aroma and fragrance in the product after high temperature is very large, which seriously affects the taste of the product
The second is that the duration of cool feeling of menthol in people's skin and oral cavity is shorter
However, the application of supramolecular controlled-release cooling flavor to the cigarette field has not yet been completed.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] A method for preparing a supramolecular controlled-release cool-feel flavor cigarette mouthpiece, characterized in that the specific steps are as follows:

[0023] (1) Weigh 100g of hydroxypropyl cyclodextrin, put it into a glass container, add 500g of water at a weight ratio of 1:5 (hydroxypropyl cyclodextrin: water), and stir at 30-60°C until The hydroxypropyl cyclodextrin supramolecular material is completely dissolved to obtain a supramolecular material solution;

[0024] (2) Weigh 100g of menthol, put it into another glass container, add 1kg of 70% ethanol by weight in a ratio of 1:10 (menthol: 70% aqueous ethanol), and stir until menthol Dissolve completely, obtain menthol solution;

[0025] (3) take by weight 1:8 (menthol solution: supramolecular material solution) respectively the menthol solution prepared in the step (2) of 50g and the supramolecular material solution prepared in the 400g step (1), at temperature Stir the matrix solution at 30-60°C and a rota...

Embodiment 2

[0029] A method for preparing a supramolecular controlled-release cool-feel flavor cigarette mouthpiece, characterized in that the specific steps are as follows:

[0030] (1) Weigh 100g aminoporphyrin, put it into a glass container, add 1kg mass fraction of 20% ethanol aqueous solution in a ratio of 1:10 by weight (aminoporphyrin: 20% ethanol aqueous solution), and heat the mixture at 30-60°C stirring under conditions until the aminoporphyrin supramolecular material is completely dissolved to obtain a supramolecular material solution;

[0031] (2) Weigh 100g of cooling essence, said cooling essence is prepared by peppermint oil, menthol and menthone according to the weight ratio of 1:8:1, put it into another glass container, and press the weight ratio of 1 :8 (cooling essence: 70% ethanol aqueous solution) ratio adds 800g mass fraction 60% ethanol aqueous solution, stirs until cooling essence dissolves completely, obtains cooling essence solution;

[0032] (3) Weigh the cooli...

Embodiment 3

[0036] A method for preparing a supramolecular controlled-release cool-feel flavor cigarette mouthpiece, characterized in that the specific steps are as follows:

[0037] (1) Take by weighing 100g calixarene sulfonate sodium, put it into a glass container, add 1.5kg mass fraction 60% ethanol aqueous solution in a ratio of 1:15 by weight (calixarene sulfonate: 60% aqueous ethanol solution), Stirring at 30-60°C until the calixarene sodium sulfonate supramolecular material is completely dissolved to obtain a supramolecular material solution;

[0038] (2) The borneol of 100g is weighed, put into another glass container, add the ethanol aqueous solution of 1.5kg mass fraction 70% by weight ratio 1:15 (borneol: 70% ethanol aqueous solution), stir until borneol The brain is completely dissolved to obtain a borneol solution;

[0039] (3) Take by weight 1:10 (borneol solution: supramolecular material solution) respectively the borneol solution prepared in 100g step (2) and the supramole...

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Abstract

The invention provides a preparation method of a cigarette tip rod with supramolecular controlled-release cool essence. The preparation method comprises the following specific steps that a supramolecular material and an aqueous ethanol solution with the mass fraction of 0%-95% are mixed according to the weight ratio of 1:0.5-1:30 and stirred to form a supramolecular material solution, and the cool essence and an aqueous ethanol solution with the mass fraction of 50%-95% are stirred to be uniform according to the weight ratio of 1:0.5-1:30 to obtain a cool essence solution; the cool essence solution and the supramolecular material solution are mixed and stirred according to the weight ratio of 1:0.5-1:30, homogenized and then applied to tobacco shreds in the tobacco shred shaping process, and the cigarette tip rod with the supramolecular controlled-release cool essence is prepared. According to the preparation method, the essence is slowly and continuously released in the cigarette smoking process, therefore, the cigarette smoking comfortableness is improved, and harm of cigarettes to the human body health is reduced.

Description

technical field [0001] The invention belongs to the technical field of tobacco, and in particular relates to a method for preparing a cigarette mouthpiece with supramolecular controlled-release cooling essence. Background technique [0002] Because the cool essence is widely used in daily chemicals, food, tobacco, medicine and personal hygiene products, it has been paid attention to by people for a long time. Natural menthol is one of the most widely used spices in cool flavors. It is always favored by people because of its low price, pure taste, safety and easy availability. With the continuous improvement of people's requirements for cool products, the shortcomings and deficiencies of menthol are gradually exposed, which are mainly manifested in two aspects. One is in terms of high temperature resistance. , especially the loss of aroma and fragrance in the product after high temperature is very large, which seriously affects the taste of the product. The 2nd, the cool fe...

Claims

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Application Information

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IPC IPC(8): A24D3/02A24D3/06A24D3/10C11B9/02
CPCA24D3/02A24D3/061A24D3/062A24D3/10C11B9/022C11B9/025
Inventor 王娜熊国玺司辉谢豪张耀华庞哲王萍张敦铁
Owner HUBEI CHINA TOBACCO IND
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